4.7 Article

Effect of tetragonal zirconia nanoparticle content on enamel strength

Journal

CERAMICS INTERNATIONAL
Volume 48, Issue 7, Pages 9710-9720

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.12.172

Keywords

Strength; Mechanical properties; ZrO2

Funding

  1. Shandong Provincial Key Laboratory
  2. Shandong Light Hydrocarbon Collaborative Innovation Center
  3. Science and Technology Plan Project of Shandong Province, China [J18KB007]
  4. Natural Science Foundation of Shandong Province [ZR2020ME132]
  5. National Natural Science Foundation of China [51971192]

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This study investigated the effect of tetragonal zirconia nanoparticles on enamel strength, and found that the addition of nano-t-ZrO2 improved surface morphology and reduced porosity of the enamel, resulting in decreased brittleness and increased strength.
The fracture failure of enamel is caused by hole-type flaws and cracks generally present in enamel. In this study, the effect of tetragonal zirconia nanoparticles (nano-t-ZrO2) on enamel strength was investigated. The addition of nano-t-ZrO2 improved the surface morphology and reduced the porosity of the enamel as determined by morphological and porosity distribution analyses. The strain on the enamel surface was recorded using a strain gauge attached to the enamel surface. The crack initiation force and strain were measured using the strain gauge, and the crack propagation diagrams at various stages of the tensile process were recorded. The relationship between the crack initiation energy and nano-t-ZrO2 content was found to be non-linear. Nano-t-ZrO2 affected the strength of the enamel. Moreover, the tensile force required for the appearance of cracks first increased and then decreased with an increase in the nano-t-ZrO2 content. The addition of nano-t-ZrO2 to the enamel matrix suppressed the formation of stress concentration regions and decreased the brittleness of the enamel. At a nano-tZrO(2) content of more than 5 wt%, the ZrO2 particles agglomerated.

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