Journal
CARBOHYDRATE RESEARCH
Volume 511, Issue -, Pages -Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2021.108489
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Funding
- Max-Planck Society
- Deutsche Forschungsgemeinschaft [DFG SFB 1449]
- Alexander von Humboldt Foundation
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The toolbox for the functionalization of glycans assembled on solid-phase is currently limited. This study presents automated and manual phosphorylation protocols for the solid-phase synthesis of oligosaccharides containing up to two mannose-6-phosphates. Automated glycan assembly allows fast access to substrates and facilitates the screening of experimental conditions.
Currently, the reaction toolbox for the functionalization of glycans assembled on solid-phase is quite limited. Automated (1 h) and manual (overnight) phosphorylation protocols that enable the solid-phase synthesis of oligosaccharides containing up to two mannose-6-phosphates are presented. Automated glycan assembly expedited access to substrates and facilitated the screening of experimental conditions.
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