Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 364, Issue 3, Pages 574-580Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.202101012
Keywords
Visible-light-induced; Heterogeneous catalysis; beta, gamma-Unsaturated oximes; Isoxazolines
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Funding
- National Natural Science Foundation of China [21971224, 22071222]
- Key Research Projects of Universities in Henan Province [20A150006, 21A150053]
- Natural Science Foundation of Henan Province [202300410375]
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A method using graphitic carbon nitride (g-C3N4) as a heterogeneous photocatalyst for the synthesis of diverse isoxazolines with a hydroxyl moiety was developed, showing advantages such as step economy, easy operation, recyclable photocatalyst, absence of external reductant/oxidant, and mild reaction conditions. Mechanistic studies revealed the generation of hydroxyl radicals under the photocatalysis of g-C3N4.
A visible-light-induced dioxygenation of beta, gamma-unsaturated oximes for the synthesis of diverse useful isoxazolines bearing a hydroxyl moiety was developed by employing graphitic carbon nitride (g-C3N4) as a heterogeneous photocatalyst under an air atmosphere. Noted that, the eminent advantages of this metal-free protocol include step economy, easy operation, a recyclable photocatalyst, external reductant-/oxidant-free and mild reaction conditions. Additionally, mechanistic studies indicated hydroxyl radical was generated under the photocatalysis of g-C3N4.
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