4.1 Article Data Paper

2D Raman, ATR-FTIR, WAXD, SAXS and DSC data of PET mono- and PET/PA6 bicomponent filaments

Journal

DATA IN BRIEF
Volume 38, Issue -, Pages -

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ELSEVIER
DOI: 10.1016/j.dib.2021.107416

Keywords

Raman mapping; PET fibers; X-ray diffraction; Infrared spectroscopy; Crystallinity; Radial gradients

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This study provides a detailed analysis of the structural data of poly(ethylene terephthalate) (PET) monofilaments and PET-polyamide 6 (PA6) filaments using various analytical techniques, including Raman mapping, attenuated total reflection Fourier transform infrared spectroscopy, wide-angle x-ray diffraction, small-angle x-ray scattering, differential scanning calorimetry, and atomic force microscopy imaging.
This data in brief article summarizes structural data obtained from monocomponent melt-spun and offline drawn poly(ethylene terephthalate) (PET) monofilaments, as well as from melt-spun bicomponent core-sheath PET-polyamide 6 (PA6) filaments. The diameters of the single filaments range from 27 mu m to 79 mu m. Presented analysis techniques and results thereof are (i) Raman mapping of filament crosssections: 2D maps of peak positions, widths, peak area ratios; (ii) attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR): ATR-FTIR spectra and extraction of surface crystallinity; (iii) wide-angle x-ray diffraction (WAXD): WAXD patterns and extraction of average crystallinity; (iv) small-angle x-ray scattering (SAXS): SAXS patterns and determined crystallite sizes and long-spacings; (v) differential scanning calorimetry (DSC): thermograms and extracted average crystallinity as well as thermal properties; (vi) atomic force microscopy (AFM): AFM image of the surface of an embedded fiber cross-section. For more information, see the publication by E. Perret et al. 'High-resolution 2D Raman mapping of mono-and bicomponent filament cross-sections' [1] . (C) 2021 The Authors. Published by Elsevier Inc.

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