4.6 Article

Evaluation of Adhesion Properties of Hard Coatings by Means of Indentation and Acoustic Emission

Journal

COATINGS
Volume 11, Issue 8, Pages -

Publisher

MDPI
DOI: 10.3390/coatings11080919

Keywords

adhesion; coatings; thin films; testing; mechanical properties; indentation; acoustic emission

Funding

  1. Slovak Research and Development Agency [APVV-15-0168]
  2. Slovak Republic Scientific Grant Agency (VEGA) [1/0540/19]
  3. Operational Programme Research and Innovation for the project: Scientific and Research Centre of Excellence SlovakION for Material and Interdisciplinary Research [ITMS2014+: 313011W085]
  4. European Regional Development Fund

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A novel method combining static indentation and acoustic emission signal detection was used in this study to evaluate the wear and adhesion of coatings. A special measuring device equipped with an acoustic emission measuring gauge was developed for this purpose, allowing the investigation of crack formation and adhesion of coatings deposited on different substrates using acoustic emissions data. The results obtained from both the existing and novel methods were compared and evaluated.
In general, the mechanical properties of hard thin coatings are investigated using indentation methods. Material characteristics of hard coatings, such as elastic modulus and hardness, are evaluated by means of nanoindentation and an appropriate evaluation methodology. The most popular method used to obtain the coating properties required using nanoindentation is the evaluation based on the Oliver and Pharr methodology. Adhesion and wear properties can be calculated using these data. In this study, we used a novel method to evaluate the wear and adhesion of coatings. A special measuring device combined with static indentation and acoustic emission signal detection was developed to evaluate the adhesion of coatings. The device consists of a macrohardness instrumental indentation device equipped with an acoustic emission measuring gauge. It was used to investigate crack formation and adhesion of coatings deposited on different substrates using acoustic emissions data. The results using both the existing and novel methods were compared and evaluated.

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