4.7 Article

Production and characterization of laser cladding coating of Fe66Co7Nb4B23 (at.%) gas-atomized and ball-milled powders

Journal

JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
Volume 14, Issue -, Pages 2267-2280

Publisher

ELSEVIER
DOI: 10.1016/j.jmrt.2021.07.087

Keywords

Fe-based alloy; Gas atomization; High-energy ball milling; Glassy phase; Laser cladding; Coating

Funding

  1. Instituto Federal de Sao Paulo (IFSP)
  2. Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior -Brazil (CAPES) [001]
  3. FAPESP (Sao Paulo State Research Foundation) [2013/05987-8]

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A new Fe66Co7Nb4B23 (at.%) alloy was produced and used to create laser cladding coatings. Optimization of parameters resulted in the successful production of high microhardness and dense coatings, demonstrating the potential for producing protective wear-resistant coatings on conventional steel components.
In this study, a new Fe66Co7Nb4B23 (at.%) alloy was produced from commercially graded precursors. Gas atomized powder of this alloy was produced, and coarser particles (splat plates, size ranges 5 cm) were subsequently submitted to high-energy ball milling. Laser cladding coating of Fe66Co7Nb4B23 (at.%) gas-atomized and ball milled powders was produced. Powders and laser cladding coatings were characterized by differential scanning calorimetry (DSC), X-ray diffraction (XRD) and scanning electron microscopy (SEM). Gas atomized and ball milled Fe66Co7Nb4B23 (at.%) powders showed a glassy matrix with some crystalline phases such as alpha-(Fe,Co) and Fe- and Co-containing borides. Both were employed as feedstock powders (<45 mm) to produce single tracks and laser cladding (LC) coating. Optimizing of the LC parameters allowed to obtain and to evaluate single tracks, aiming the production of LC coatings from the optimized parameters. The single tracks were composed of alpha-(Fe,Co), M2B and M3B phases, and displayed high microhardness, ranging from of 980 +/- 150 to 1480 +/- 70 HV0.5, depending on the powder and LC parameters. The resulting LC coatings were dense and free from excessive defects such as cracks, porosity and insufficient metallurgical bonding to the AISI 1020 steel substrate. These findings open perspectives to produce protective wear-resistant and affordable coatings on conventional steel components. (C) 2021 The Authors. Published by Elsevier B.V.

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