Journal
MATERIALS & DESIGN
Volume 206, Issue -, Pages -Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.matdes.2021.109826
Keywords
Cold spraying (CS); Annealing; Strength-ductility; Crack growth behavior; In-situ SEM tensile testing
Categories
Funding
- Alexander von Humboldt Foundation
- European Research Council [716678]
- Fonds de la recherche scientifique-FNRS (FRIA grant), Belgium
- National Natural Science Foundation of China [52061135101, 52001078]
- Guangdong Basic and Applied Basic Research Foundation [2019B1515120016]
- Key-Area Research and Development Program of Guangdong Province [2020B0101330001]
- European Research Council (ERC) [716678] Funding Source: European Research Council (ERC)
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By appropriately annealing metallic deposits manufactured by cold spraying, the strength and fracture strain can be significantly improved. Copper has been identified as a reliable material for cold spraying, and assessing the strength of copper powder can help correlate deposit strength with process parameters and material properties. In-situ observations during tensile testing can provide insights into crack initiation, growth, and final fracture, revealing failure mechanisms and allowing for the identification of solutions for improving cold-sprayed deposits.
Low ductility of metallic deposits manufactured by cold spraying (CS) impedes potential mechanical performances in industrial applications. Through appropriate annealing treatment, the amount of both, non bonded interfaces and work hardening promoted dislocations during CS can be significantly reduced. Consequently, the annealed samples exhibit higher strength and fracture strain than the as-deposited ones. Cu was selected as a reliable material for CS. To correlate Cu deposit strength with primary process parameters and material properties, the Cu powder strength was assessed. Crack characterization of Cu deposits was performed by in-situ microscopic observations during tensile testing. The direct observation of crack initiation, growth and final fracture allows revealing failure mechanisms. The in-situ tests allow distinguishing the effects of reduced initial defect sizes due to annealing and improved ductility in the vicinity of initial defects on possible crack growth and part failure. Considering the necessary compromise between strength, uniform elongation, ductility and microhardness, a post-spraying annealing process is desirable for CSed Cu deposits. The identification of macroscopic and micro-mechanical properties attained under respective process parameters and influences of annealing processes therefore allow identifying solutions for improvements of CSed deposits for load-carrying applications, which is a prerequisite for using CS as additive manufacturing technique. (c) 2021 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY license (http:// creativecommons.org/licenses/by/4.0/).
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