4.6 Article

Automatic Identification and Quantitative Characterization of Primary Dendrite Microstructure Based on Machine Learning

Journal

CRYSTALS
Volume 11, Issue 9, Pages -

Publisher

MDPI
DOI: 10.3390/cryst11091060

Keywords

single crystal superalloy; TTA Faster R-CNN; PDAS; local multi-direction; Voronoi tessellation

Funding

  1. National Key Research and Development Program of China [2017YFB0702100]

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A method for automatically detecting dendrite cores and calculating local PDAS in single-crystal superalloys was proposed in this study. By utilizing the Faster R-CNN algorithm and TTA technology, the accuracy reached 98.4% and successfully captured the Gaussian distribution of local PDAS, enabling rapid, accurate, and quantitative characterization of dendritic distribution.
Dendrites are important microstructures in single-crystal superalloys. The distribution of dendrites is closely related to the heat treatment process and mechanical properties of single-crystal superalloys. The primary dendrite arm spacing (PDAS) is an important length scale to describe the distribution of dendrites. In this work, the second-generation single crystal superalloy HT901 with a diameter of 15 mm was imaged under a metallurgical microscope. An automatic dendrite core identification and full-field quantitative statistical analysis method is proposed to automatically detect the dendrite core and calculate the local PDAS. The Faster R-CNN algorithm combined with test time augmentation (TTA) technology is used to automatically identify the dendrite cores. The local multi-directional algorithm combined with Voronoi tessellation is used to determine the local nearest neighbor dendrite and calculate the local PDAS and coordination number. The accuracy of using Faster R-CNN combined with TTA to detect the dendrite core of HT901 reaches 98.4%, which is 15.9% higher than using Faster R-CNN alone. The algorithm calculates the local PDAS of all dendrites in H901 and captures the Gaussian distribution of the local PDAS. The average PDAS determined by the Gaussian distribution is 415 mu m, which is only a small difference from the average spacing lambda over bar (420 mu m) calculated by the traditional method. The technology analyzes the relationship between the local PDAS and the distance from the center of the sample. The local PDAS near the center of HT901 are larger than those near the edge. The results suggests that the method enables the rapid, accurate and quantitative dendritic distribution characterization.

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