4.5 Article

The Effect of Solidification Rate on the Microstructure and Mechanical Properties of Pure Magnesium

Journal

METALS
Volume 11, Issue 8, Pages -

Publisher

MDPI
DOI: 10.3390/met11081264

Keywords

magnesium; microstructure of magnesium; mechanical properties of magnesium; solidification of pure magnesium; quenching

Funding

  1. University of Wisconsin-Milwaukee
  2. H.H. Harris Foundation
  3. Minerals-Metals-Materials Society (TMS)
  4. American Institute of Mining-Metallurgical-Petroleum Engineers (AIME)
  5. Foundry Educational Foundation (FEF)-Northeastern Wisconsin-George J. Barker Memorial
  6. American Foundry Society (AFS)
  7. Association for Iron & Steel Technology (AIST)

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The research investigated the influence of different cooling rates on the strength of pure Mg, finding that increasing the solidification rate can enhance hardness and ultimate tensile strength. In addition, improving grain structure can help to improve the mechanical properties of the material.
Magnesium, Mg, has been widely investigated due to its promising potential as magnesium alloys for various applications, particularly as biomedical implantation devices among other medical applications. This work investigates the influence of different cooling rates on the strength of pure Mg. The cooling rates were set to cover a low cooling rate LCR (0.035 degrees C/s) in an insulated furnace, a moderate cooling rate MCR (0.074 degrees C/s) in uninsulated-ends furnace, and a high cooling rate HCR (13.5 degrees C/s) in liquid CO2. The casting process was accomplished using a closed system of melting and cooling due to the reactivity-flammability of magnesium in order to minimize processing defects and increase the safety factor. The as-cast samples were metallographically examined for their microstructure, and properties such as impact strength, hardness, and tension were determined. Increasing the solidification rate from 0.035 degrees C/s to 0.074 degrees C/s increased the hardness from 30 to 34 Rockwell Hardness and the UTS from 48 to 67 MPa. A higher solidification rate of 13.5 degrees C/s further enhanced the hardness to 48 Rockwell Hardness and the UTS to 87 MPa in comparison to the 0.074 degrees C/s cooling rate. Additionally, the fracture behavior and morphology were investigated. It was found that in general, the mechanical properties tended to improve by refining the grain structure.

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