Journal
ORGANIC LETTERS
Volume 23, Issue 15, Pages 6153-6157Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.1c02275
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Funding
- National Natural Science Foundation of China [21101085]
- Natural Science Foundation of Liaoning Province [2015020196]
- Liaoning Revitalization Talents Program [XLYC1902085]
- PetroChina Innovation Foundation [2018D-5007-0507]
- Research Project Fund of Liaoning Provincial Department of Education [L2019037]
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An efficient visible-light-promoted N-radical-mediated tandem radical cyclization/defluorinated alkylation of beta,gamma-unsaturated hydrazones and alpha-trifluoromethyl alkenes was described. This protocol provides a general and effective route to synthesize various dihydropyrazole-fused gem-difluoroalkenes at moderate to excellent yields under redox-neutral, metal-free, and mild conditions.
An efficient visible-light-promoted N-radical-mediated tandem radical cyclization/defluorinated alkylation of beta,gamma-unsaturated hydrazones, and alpha-trifluoromethyl alkenes is described. This protocol provides a general and effective route to synthesize various dihydropyrazole-fused gem-difluoroalkenes at moderate to excellent yields under redox-neutral, metal-free, and mild conditions.
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