Effect of annealing temperature on structure and high-temperature soft magnetic properties of (Fe0.9Co0.1)72.7Al0.8Si13.5Cu1Nb3B8V1 nanocrystalline alloy

The structure and soft magnetic properties of nanocrystalline (Fe0.9Co0.1)(72.7)Al0.8Si13.5Cu1Nb3B8V1 alloy annealed at 510-690 degrees C were investigated by XRD patterns and initial permeability. It was observed that annealing within the ranges of 510-630 degrees C, only soft magnetic crystalline phase precipitated from the amorphous matrix. With the increase of annealing temperature, the grain size (D) and volume fraction of the crystalline phase (V-cry) both gradually increase from 11.9 nm to 13.7 nm and from 58 % to 89 % respectively. In the meanwhile, the thickness of the amorphous layer (Lambda) gradually decreases from 2.37 nm to 0.54 nm. The change of initial permeability with temperature (mu i -T curves) showed that the mu i declines with increasing temperature. However, the rate of descent is different and the higher annealing temperature (T-a) corresponds to the slower attenuation of mu i. The high-temperature mu i gradually improves with annealing temperature (Ta) increasing up to 630 degrees C, and the higher mu i of 1500 can be held up to 600 degrees C. However, the high-temperature mu i dramatically deteriorates after annealing at 690 degrees C due to the precipitating hard magnetic phase from the residual amorphous matrix.

Automated summary

Investigation of the structure and soft magnetic properties of nanocrystalline (Fe0.9Co0.1)(72.7)Al0.8Si13.5Cu1Nb3B8V1 alloy annealed at 510-690 degrees C revealed that with increasing annealing temperature, grain size and volume fraction of the crystalline phase increased while the thickness of the amorphous layer decreased. Higher annealing temperatures resulted in improved high-temperature initial permeability up to 630 degrees C, but a dramatic deterioration was observed at 690 degrees C due to the precipitation of hard magnetic phase.