4.5 Article

Surface properties of a new lithium disilicate glass-ceramic after grinding

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Publisher

SPRINGER
DOI: 10.1007/s10856-021-06592-w

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Funding

  1. Coordination for the Improvement of Higher Education Personnel (CAPES)
  2. Sao Paulo Research Foundation (FAPESP) through the Center for Research, Technology and Education in Vitreous Materials (CeRTEV) [2013/07793-6]

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Grinding was found to smooth the surfaces of both LaMaV Press and IPS e-max Press without significantly altering their hardness and surface energy. Both materials exhibited similar surface properties when subjected to clinical adjustments.
This study aimed to evaluate the effect of grinding on some surface properties of two lithium disilicate-based glass-ceramics, one experimental new product denominated LaMaV Press (UFSCar-Brazil) and another commercial known as IPS e-max Press (Ivoclar), in the context of simulated clinical adjustment. Discs (N = 24, 12 mm in diameter) were separated into four groups: LaMaV Press with no grinding (E), LaMaV Press after grinding (EG), IPS e-max Press with no grinding (C), and IPS e-max Press after grinding (CG). A 0.1-mm deep grinding was carried out on EG and CG samples (final thickness of 1.4 mm) using a diamond stone in a low-speed device. The E and C samples had the same thickness. The effect of grinding on the sample surfaces was evaluated by X-ray diffraction, mechanical and optical profilometry, scanning electron microscopy, goniometry, and Vickers hardness. The mean roughness (Ra) was evaluated by Kruskal-Wallis and Student-Newman-Keuls statistics. The surface energy (SE) by the sessile drop method and Vickers hardness (VH) were analyzed using two-way ANOVA. The Ra medians were E = 1.69 mu m, EG = 1.57 mu m, C = 1.45 mu m, and CG = 1.13 mu m with p = 0.0284. The SE and VH were similar for all materials and treatments. Grinding smoothed the surfaces and did not significantly alter the hardness and surface energy of both LaMaV Press and IPS e-max Press. These glass-ceramics presented similar surface properties, and clinical adjustments can be implemented without loss of performance of both materials. A grinding standardization device developed that allowed to control the amount of grinding, the speed of rotation speed and the force exerted on the samples. [GRAPHICS]

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