Journal
FOOD CHEMISTRY
Volume 190, Issue -, Pages 20-24Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2015.05.076
Keywords
Chemiluminescence; Flow-injection; Potassium bromate; Flour
Funding
- natural science foundation of Jiangsu Province Youth Fund [BK20130646]
- Research and Innovation Project for Graduate Students Academic Degree of Colleges and Universities of Jiangsu Province [KYZZ0185]
- Fundamental Research Funds for the Central Universities [JKPZ2013017]
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A novel and highly sensitive flow-injection chemiluminescence method for the determination of potassium bromate (KBrO3) has been developed. This method is based on the luminescence properties of the KBrO3-Na2SO3-quinine sulfate system in acid medium. Optimized experimental conditions and a possible mechanism were investigated. The relative chemiluminescence intensity responded linearly to the concentration of KBrO3 in the range of 7.054 x 10(-6)-1.008 x 10(-4) mol/L with a detection limit of 2.116 x 10(-6) mol/L. The relative standard deviation (RSD) at 5.0 x 10(-5) mol/L KBrO3 (n = 12) was 2.3%. The proposed method was applied successfully to the determination of KBrO3 in flour. (C) 2015 Elsevier Ltd. All rights reserved.
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