☆ 4.8 Review

Technological Innovations in Photochemistry for Organic Synthesis: Flow Chemistry, High-Throughput Experimentation, Scale-up, and Photoelectrochemistry

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Copper-Photocatalyzed Hydroboration of Alkynes and Alkenes

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Recent Development of Aryl Diazonium Chemistry for the Derivatization of Aromatic Compounds

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Chemical Aspects of Human and Environmental Overload with Fluorine

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Organophotocatalytic Aerobic Oxygenation of Phenols in a Visible-Light Continuous-Flow Photoreactor

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Summary: A mild photocatalytic phenol oxygenation process using visible light and pressurized air was described, enabling high yields of products for various applications including vitamin synthesis by controlling key process parameters. The reactor design allows for low organophotocatalyst loadings to generate singlet oxygen, contributing to sustainable synthesis of benzoquinones and p-quinols through efficient aerobic phenol oxygenation.

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In situ chloride-mediated synthesis of TiO2 thin film photoanode with enhanced photoelectrochemical activity for carbamazepine oxidation coupled with simultaneous cathodic H2 production and CO2 conversion to fuels

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JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Fluorinated Ketones as Trapping Reagents for Visible-Light-Induced Singlet Nucleophilic Carbenes

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Review Chemistry, Multidisciplinary

Scalability of photochemical reactions in continuous flow mode

Kian Donnelly et al.

Summary: Continuous flow photochemistry has become increasingly popular in both academia and industry over the last decade due to its safety, practicality, and ability to rapidly access complex chemical structures. The development of new energy efficient LED lamps and innovative reactor designs has further enhanced the practicality and productivity of modern photochemical flow reactors.

JOURNAL OF FLOW CHEMISTRY (2021)

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Article Chemistry, Physical

Photocatalytic Oxygenation of Heterostilbenes-Batch versus Microflow Reactor

Milena Mlakic et al.

Summary: The photocatalytic oxygenation of novel furo- and thieno heterostilbenes with water-soluble manganese(III) porphyrins allowed for the study of reactivities and reaction pathways dependent on heteroatoms and catalyst charges, with faster reactions observed in microflow reactors due to more favorable mass transfer, diffusion, and light penetration conditions.

CATALYSTS (2021)

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Article Engineering, Environmental

Visible-light photooxidation of benzene to phenol in continuous-flow microreactors

Xiaoqi Shi et al.

Summary: In this study, phenol was successfully synthesized through photooxidation, reaching a high yield of 94% and selectivity over 99% under optimized conditions. The photomicroreactor with blue LEDs as an eco-friendly light source demonstrated significant advantages, while a reaction kinetic model was established to further understand the photooxidation mechanism.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Chemistry, Multidisciplinary

Copper-Photocatalyzed Hydrosilylation of Alkynes and Alkenes under Continuous Flow

Mingbing Zhong et al.

Summary: This paper describes the photocatalytic hydrosilylation of alkynes and alkenes under continuous flow conditions using a specific catalyst and blue LED light, resulting in good to excellent yields for a variety of alkenes and alkynes with high functional group tolerance. The reaction mechanism was studied, and a plausible scenario was proposed.

CHEMISTRY-A EUROPEAN JOURNAL (2021)

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Article Chemistry, Multidisciplinary

C-H Amination via Electrophotocatalytic Ritter-type Reaction

Tao Shen et al.

Summary: A method for C-H bond amination via electrophotocatalytic Ritter-type reaction has been developed, catalyzed by a trisaminocyclopropenium (TAC) ion in an electrochemical cell under irradiation, converting benzylic C-H bonds to acetamides without stoichiometric chemical oxidant. The method demonstrates compatibility with a wide range of functionalities and shows successful transformation of several complex substrates.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Article Multidisciplinary Sciences

Photocatalytic C-H activation and the subtle role of chlorine radical complexation in reactivity

Qiaomu Yang et al.

Summary: The reported carbon-hydrogen (C-H) activation of alkanes is actually mediated by the photocatalyst [NEt4](2)[CeCl6], and RO center dot are not intermediates. The generation of chlorine radical (Cl center dot) in the photocatalytic system is found to be the rate-limiting step. Density functional theory calculations support the formation of [Cl center dot][alcohol] adducts, which can manifest a masked RO center dot character.

SCIENCE (2021)

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Article Chemistry, Multidisciplinary

Rapid Optimization of Photoredox Reactions for Continuous-Flow Systems Using Microscale Batch Technology

Maria Gonzalez-Esguevillas et al.

Summary: This study introduces a new method that utilizes a microscale high-throughput experimentation platform to identify optimal reaction conditions that can be directly translated to flow systems. By simulating the flow-vessel pathway within a microscale reaction plate, the rapid identification of optimal flow reaction conditions is enabled, and this method has been validated to accurately translate to commercial flow reactors.

ACS CENTRAL SCIENCE (2021)

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Article Chemistry, Multidisciplinary

Combining machine learning and high-throughput experimentation to discover photocatalytically active organic molecules

Xiaobo Li et al.

Summary: Organic molecules play a crucial role in photocatalysts, but reliable structure-property design rules are difficult to formulate. By integrating experiment, computation, and machine learning, researchers were able to identify common structural features in molecules with high catalytic activity. The study marks a step towards the machine-learning assisted discovery of molecular organic photocatalysts, with potential applications beyond photocatalytic hydrogen evolution.

CHEMICAL SCIENCE (2021)

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Article Chemistry, Multidisciplinary

A highly selective decarboxylative deuteration of carboxylic acids

Nian Li et al.

Summary: This paper presents a mild and practical method for precise deuterium incorporation in aliphatic carboxylic acids using synergistic photoredox and HAT catalysis. The reaction shows excellent D-incorporation even in substrates with reactive C-H bonds or versatile functional groups, and can be scaled up to 50 mmol under very mild conditions. Precision deuteration of readily available complex carboxylic acids makes this protocol promising for the preparation of deuterium-labeled compounds.

CHEMICAL SCIENCE (2021)

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Review Chemistry, Organic

Fluorination and fluoroalkylation of alkenes/alkynes to construct fluoro-containing heterocycles

Xin Wang et al.

Summary: Fluoro-containing heterocycles are widely used in various fields due to their unique properties, leading to a rapid development in the research of new synthetic methods for these compounds. This review summarizes established strategies for constructing fluoro-containing heterocycles over the past decade, highlighting the scopes, mechanisms, unsolved issues, and future directions in this field.

ORGANIC CHEMISTRY FRONTIERS (2021)

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Review Chemistry, Multidisciplinary

From circular synthesis to material manufacturing: advances, challenges, and future steps for using flow chemistry in novel application area

Alessandra Sivo et al.

Summary: Continuous-flow technologies have shown great potential in the chemistry field, particularly in drug discovery and drug development. However, there is still room for improvement in other areas such as circular valorization of waste products and manufacturing of materials and catalysts.

REACTION CHEMISTRY & ENGINEERING (2021)

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Article Chemistry, Multidisciplinary

A photochemical ring expansion of 6-to 8-membered nitrogen heterocycles by [1,3]-sigmatropic rearrangement

Morgan A. Manning et al.

Summary: A new route to azocines and benzoazocines from furopyridinones is described through a photochemically induced [1,3]-sigmatropic rearrangement. The method provides excellent atom economy by sequencing thermal and photochemical ring expansion steps under continuous flow.

CHEMICAL COMMUNICATIONS (2021)

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Review Chemistry, Multidisciplinary

Ready, Set, Flow! Automated Continuous Synthesis and Optimization

Christopher P. Breen et al.

Summary: Synthetic chemistry has opened up new possibilities for innovation in key industries such as medicine, energy, and agriculture. Automation is challenging the traditional process of chemical synthesis, while continuous flow chemistry presents a flexible platform for automation. The merger of synthesis and automation is expected to democratize access to custom complex small molecules and accelerate the development of new synthetic protocols.

TRENDS IN CHEMISTRY (2021)

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Article Chemistry, Multidisciplinary

Evaluation of a Continuous-Flow Photo-Bromination Using N-Bromosuccinimide for Use in Chemical Manufacture

Matthew Waterford et al.

Summary: By utilizing a flow reactor system, it is possible to independently control light intensity, wavelength, and reaction temperature, thereby enhancing control over the reaction. The study demonstrated that under specific conditions, the target product can be efficiently synthesized, and this easy-to-handle reaction system has the potential for scaled-up production.

AUSTRALIAN JOURNAL OF CHEMISTRY (2021)

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Article Chemistry, Multidisciplinary

Photoelectrochemical cross-dehydrogenative coupling of benzothiazoles with strong aliphatic C-H bonds†

Luca Capaldo et al.

Summary: A novel photoelectrochemical strategy was developed for the cross-dehydrogenative coupling of unactivated aliphatic hydrogen donors with benzothiazoles. By using a specific photocatalyst to activate strong C(sp(3))-H bonds in the substrates, while utilizing electrochemistry to scavenge extra electrons, the reaction was efficiently achieved.

CHEMICAL COMMUNICATIONS (2021)

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Review Chemistry, Multidisciplinary

Hexafluoroisopropanol: the magical solvent for Pd-catalyzed C-H activation

Trisha Bhattacharya et al.

Summary: HFIP, as a solvent, plays a unique role in Pd-catalyzed C-H functionalization reactions, especially in enhancing yield and selectivity, making it irreplaceable.

CHEMICAL SCIENCE (2021)

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Review Chemistry, Multidisciplinary

Visible light photocatalysis in the late-stage functionalization of pharmaceutically relevant compounds

Rolando Cannalire et al.

Summary: Late stage functionalization is a powerful tool for accelerating the identification of structure-activity relationships and optimizing ADME profiles of drugs. Visible-light photocatalysis offers a smooth and clean functionalization approach for drugs, with a critical assessment of current literature and highlighting expected future progress and potential applications in the field.

CHEMICAL SOCIETY REVIEWS (2021)

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Article Chemistry, Multidisciplinary

A continuous flow synthesis of [1.1.1]propellane and bicyclo[1.1.1]pentane derivatives

Kian Donnelly et al.

Summary: This study presents a continuous flow process for on-demand generation of [1.1.1]propellane, providing solutions for direct derivatization into various BCP species, with throughputs up to 8.5 mmol h(-1) and access to gram quantities of selected BCP building blocks. Lastly, a continuous photochemical transformation method was developed to convert [1.1.1]propellane into valuable BCPs bearing mixed ester/acyl chloride moieties.

CHEMICAL COMMUNICATIONS (2021)

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Article Engineering, Environmental

An Overview of Photoreactors and Computational Modeling for the Intensification of Photocatalytic Processes in the Gas-Phase: State-of-Art

Jessica Oliveira de Brito Lira et al.

Summary: This article provides a comprehensive review of photoreactors for gas-phase reactions, focusing on process intensification and recent computer simulations. It highlights the importance of two photocatalytic gas-phase reactions, VOCs oxidation, and NOx degradation, from both scientific and social perspectives, while also acknowledging the challenges of achieving high performance due to issues like mass transfer and low quantum efficiency. Various designs of photoreactors have been explored to enhance mass and photon transfer, with emphasis on process intensification through the improved performance in these aspects.

JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING (2021)

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Review Chemistry, Multidisciplinary

Powering the next industrial revolution: transitioning from nonrenewable energy to solar fuels via CO2 reduction

Rami J. Batrice et al.

Summary: The article discusses recent advances in photochemical solar fuel production technology, emphasizing the importance of converting carbon dioxide and water into liquid fuels, and categorizing various methods into four major categories.

RSC ADVANCES (2021)

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Review Chemistry, Physical

Cooperative photoredox and palladium catalysis: recent advances in various functionalization reactions

Maniklal Shee et al.

Summary: The recent resurgence of synergistic palladium and visible-light-induced photoredox catalysis has transformed Pd-catalyzed organic synthesis by enabling unconventional bond formation modes and accessing various elusive reaction pathways under mild conditions. The combination of suitable photocatalysts with active Pd catalysts has been utilized to create efficient dual catalytic systems for cross-coupling reactions, leading to enhancements in reaction rate, conditions, functional group compatibility, and substrate scopes. This Minireview discusses the advances in cooperative catalytic reactions, showcasing their unique mechanistic features and selective examples for substrate scopes.

CATALYSIS SCIENCE & TECHNOLOGY (2021)

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Article Chemistry, Multidisciplinary

Continuous-flow step-economical synthesis of thiuram disulfides via visible-light photocatalytic aerobic oxidation

Hao-Xing Xu et al.

Summary: A continuous-flow photocatalytic synthesis method has been developed for the industrially important thiuram disulfides, using O-2 as the oxidant and Eosin Y as the photoredox catalyst. This method offers reduced reaction time, excellent product yield, and purity, making it a sustainable and potentially scalable process for industrial production.

GREEN CHEMISTRY (2021)

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Review Chemistry, Organic

Modern approaches towards the synthesis of geminal difluoroalkyl groups

Dayanne R. Carvalho et al.

Summary: This review covers the importance of and most recent approaches toward geminal difluoroalkyl groups, with special emphasis on applications to biologically-relevant compounds. Various methods such as transition metal-mediated, photochemical, and organocatalytic approaches will be discussed along with their mechanistic implications.

ORGANIC & BIOMOLECULAR CHEMISTRY (2021)

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Review Chemistry, Multidisciplinary

Toward Machine Learning-Enhanced High-Throughput Experimentation

Natalie S. Eyke et al.

Summary: Recent research indicates that machine learning (ML) and high throughput experimentation (HTE) have gained significant attention in the fields of chemistry and engineering, leading to the development of powerful reactivity models and platforms capable of rapidly executing numerous reactions. Although the integration of ML with HTE has not been fully realized, recent developments suggest the potential benefits of their combination, highlighting their complementary nature while also identifying obstacles that need to be overcome for maximizing the impact of this merger on chemical research.

TRENDS IN CHEMISTRY (2021)

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Article Chemistry, Organic

Development of a Continuous Photochemical Benzyne-Forming Process

Cormac Bracken et al.

Summary: A new methodology utilizing a high-power LED lamp for the safe generation and derivatization of benzyne under photochemical conditions is presented. The continuous-flow process effectively controls the release of gaseous by-products and delivers a series of heterocyclic products in a short residence time. This robust methodology enables the rapid generation of important heterocyclic scaffolds through a simple and scalable flow protocol.

SYNOPEN (2021)

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Article Chemistry, Multidisciplinary

Photochlorination of toluene - the thin line between intensification and selectivity. Part 2: selectivity

Umit Tastan et al.

Summary: Photochemical reactions, such as light-driven side-chain chlorination of aromatic compounds, are essential in the chemical industry. Reoptimising reaction conditions using advanced reactor designs and irradiation techniques is crucial for economic and ecological reasons. However, enhancing reaction rate must be balanced with high selectivity for the desired target compound.

REACTION CHEMISTRY & ENGINEERING (2021)

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Article Chemistry, Organic

Decagram Synthesis of Dimethyl 1,4-Cubanedicarboxylate Using Continuous-Flow Photochemistry

Diego E. Collin et al.

Summary: This paper presents a straightforward approach to scale-up a [2+2] photocycloaddition step using home-made flow photoreactors to access dimethyl 1,4-cubanedicarboxylate in decagram-scale with satisfactory yield. The method allows for faster process time and eliminates the need for batch photoreactors. The characterisation of the photocycloadduct and its hydrates has been completed.

SYNTHESIS-STUTTGART (2021)

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Article Chemistry, Organic

Smooth Metal-Free Photoinduced Preparation of Valuable 8-Arylxanthines

Havall Othman Abdulla et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Mechanochemistry for Synthesis

Tomislav Friscic et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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Review Chemistry, Organic

Photochemical Rearrangements in Heterocyclic Chemistry

Corentin Lefebvre et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Chemistry, Organic

Metal-Free Visible-Light-Mediated Hydrotrifluoromethylation of Unactivated Alkenes and Alkynes in Continuous Flow

Anne-Laure Barthelemy et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Engineering, Chemical

A UV-LEDs based photomicroreactor for mechanistic insights and kinetic studies in the norbornadiene photoisomerization

Chong Shen et al.

AICHE JOURNAL (2020)

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Article Chemistry, Multidisciplinary

Electrophotocatalytic SNAr Reactions of Unactivated Aryl Fluorides at Ambient Temperature and Without Base

He Huang et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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Article Chemistry, Multidisciplinary

Electrochemistry Broadens the Scope of Flavin Photocatalysis: Photoelectrocatalytic Oxidation of Unactivated Alcohols

Wen Zhang et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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Review Chemistry, Organic

Synergistic Photoredox/Transition-Metal Catalysis for Carbon-Carbon Bond Formation Reactions

Maxime De Abreu et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Flow Photochemical Syntheses of trans-Cyclooctenes and trans-Cycloheptenes Driven by Metal Complexation

Jessica E. Pigga et al.

ISRAEL JOURNAL OF CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

A Survival Guide for the Electro-curious

Cian Kingston et al.

ACCOUNTS OF CHEMICAL RESEARCH (2020)

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Article Nanoscience & Nanotechnology

Visible-Light Flow Reactor Packed with Porous Carbon Nitride for Aerobic Substrate Oxidations

Mark A. Bajada et al.

ACS APPLIED MATERIALS & INTERFACES (2020)

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Review Chemistry, Multidisciplinary

Synthetic Photoelectrochemistry

Joshua P. Barham et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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Article Chemistry, Physical

High-Throughput Screening of Multimetal Sulfides-Modified g-C3N4 for Degradation of Organic Contaminations Based on Ink-Jet Printing (IJP) Technology

Sifan Bi et al.

CATALYSIS LETTERS (2020)

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Article Engineering, Chemical

CFD analysis of a luminescent solar concentrator-based photomicroreactor (LSC-PM) with feedforward control applied to the synthesis of chemicals under fluctuating light intensity

Gabriela X. de Oliveira et al.

CHEMICAL ENGINEERING RESEARCH & DESIGN (2020)

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Article Chemistry, Physical

Enabling Catalyst Discovery through Machine Learning and High-Throughput Experimentation

Travis Williams et al.

CHEMISTRY OF MATERIALS (2020)

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Review Chemistry, Multidisciplinary

Recent Advances in Continuous-Flow Enantioselective Catalysis

Tao Yu et al.

CHEMISTRY-A EUROPEAN JOURNAL (2020)

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Article Chemistry, Multidisciplinary

Electrophotocatalytic Undirected C-H Trifluoromethylations of (Het)Arenes

Youai Qiu et al.

CHEMISTRY-A EUROPEAN JOURNAL (2020)

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Article Chemistry, Multidisciplinary

Organophotocatalytic N-Demethylation of Oxycodone Using Molecular Oxygen

Yuesu Chen et al.

CHEMISTRY-A EUROPEAN JOURNAL (2020)

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Review Chemistry, Organic

[2+2] Photochemical Cycloaddition in Organic Synthesis

Debayan Sarkar et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Chemistry, Organic

Visible-Light-Induced Metal-Free Trifluoromethylselenolation of Electron-Rich Heteroarenes Using the Nucleophilic [Me4N][SeCF3] Reagent

Arnaud De Zordo-Banliat et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Review Chemistry, Organic

The Dark Side of Photocatalysis: One Thousand Ways to Close the Cycle

Luca Capaldo et al.

EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Chemistry, Organic

Development of a Continuous Flow Photoisomerization Reaction Converting Isoxazoles into Diverse Oxazole Products

Cormac Bracken et al.

JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Chemistry, Organic

Visible Light-Mediated (Hetero)aryl Amination Using Ni(II) Salts and Photoredox Catalysis in Flow: A Synthesis of Tetracaine

Boyoung Y. Park et al.

JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Chemistry, Multidisciplinary

Potent Reductants via Electron-Primed Photoredox Catalysis: Unlocking Aryl Chlorides for Radical Coupling

Nicholas G. W. Cowper et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2020)

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Article Chemistry, Multidisciplinary

Reductive Electrophotocatalysis: Merging Electricity and Light To Achieve Extreme Reduction Potentials

Hyunwoo Kim et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2020)

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Article Chemistry, Multidisciplinary

Electrophotocatalytic C-H Functionalization of Ethers with High Regioselectivity

He Huang et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2020)

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Article Chemistry, Multidisciplinary

Synthesis of Sterically Hindered Primary Amines by Concurrent Tandem Photoredox Catalysis

Michael C. Nicastri et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2020)

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Review Biochemistry & Molecular Biology

Continuous Flow Photochemistry for the Preparation of Bioactive Molecules

Mara Di Filippo et al.

MOLECULES (2020)

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Article Chemistry, Organic

Continuous Flow Enables Metallaphotoredox Catalysis in a Medicinal Chemistry Setting: Accelerated Optimization and Library Execution of a Reductive Coupling between Benzylic Chlorides and Aryl Bromides

Zachary G. Brill et al.

ORGANIC LETTERS (2020)

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Article Chemistry, Organic

Continuous Flow-Enabled Synthesis of Bench-Stable Bicyclo[1.1.1]pentane Trifluoroborate Salts and Their Utilization in Metallaphotoredox Cross-Couplings

Michael D. VanHeyst et al.

ORGANIC LETTERS (2020)

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Review Chemistry, Applied

A Perspective on Continuous Flow Chemistry in the Pharmaceutical Industry

Marcus Baumann et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2020)

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Article Chemistry, Applied

Development of a General Automated Flow Photoredox 18F-Difluoromethylation of N-Heteroaromatics in an AllinOne Synthesizer

Laura Trump et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2020)

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Article Chemistry, Applied

Scalable Continuous Vortex Reactor for Gram to Kilo Scale for UV and Visible Photochemistry

Darren S. Lee et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2020)

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Article Chemistry, Applied

Multistep Synthesis of Organic Selenides under Visible Light Irradiation: A Continuous-Flow Approach

Adrian A. Heredia et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2020)

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Article Chemistry, Organic

Robust Organic Photosensitizers Immobilized on a Vinylimidazolium Functionalized Support for Singlet Oxygen Generation under Continuous-Flow Conditions

Koichiro Masuda et al.

SYNLETT (2020)

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Article Multidisciplinary Sciences

Chemistry glows green with photoredox catalysis

Giacomo E. M. Crisenza et al.

NATURE COMMUNICATIONS (2020)

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Article Multidisciplinary Sciences

Photons as a 21st century reagent

Holly E. Bonfield et al.

NATURE COMMUNICATIONS (2020)

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Article Multidisciplinary Sciences

Heterogeneous photoredox flow chemistry for the scalable organosynthesis of fine chemicals

Can Yang et al.

NATURE COMMUNICATIONS (2020)

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Article Chemistry, Physical

Parallelized Screening of Characterized and DFT-Modeled Bimetallic Colloidal Cocatalysts for Photocatalytic Hydrogen Evolution

Eric M. Lopato et al.

ACS CATALYSIS (2020)

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Article Chemistry, Physical

Photoelectrochemical Conversion of Carbon Dioxide (CO2) into Fuels and Value-Added Products

Vignesh Kumaravel et al.

ACS ENERGY LETTERS (2020)

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Article Chemistry, Physical

CO2 Reduction to CO with 19% Efficiency in a Solar-Driven Gas Diffusion Electrode Flow Cell under Outdoor Solar Illumination

Wen-Hui Cheng et al.

ACS ENERGY LETTERS (2020)

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Article Chemistry, Multidisciplinary

Electrophotocatalytic Decarboxylative C-H Functionalization of Heteroarenes

Xiao-Li Lai et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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Article Chemistry, Multidisciplinary

Photon Equivalents as a Parameter for Scaling Photoredox Reactions in Flow: Translation of Photocatalytic C-N Cross-Coupling from Lab Scale to Multikilogram Scale

Emily B. Corcoran et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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Article Chemistry, Organic

A method to determine the correct photocatalyst concentration for photooxidation reactions conducted in continuous flow reactors

Clemens R. Horn et al.

BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Review Chemistry, Organic

Recent applications of porphyrins as photocatalysts in organic synthesis: batch and continuous flow approaches

Rodrigo Costa e Silva et al.

BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Review Chemistry, Organic

Photocatalysis with organic dyes: facile access to reactive intermediates for synthesis

Stephanie G. E. Amos et al.

BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Pushing the boundaries of C-H bond functionalization chemistry using flow technology

Sebastian Govaerts et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Oxidation of organosulfur compounds promoted by continuous-flow chemistry

Juan Pablo Colomer et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Article Chemistry, Multidisciplinary

Continuous-flow synthesis and application of polymer-supported BODIPY Photosensitisers for the generation of singlet oxygen; process optimised by in-line NMR spectroscopy

Christopher G. Thomson et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Article Chemistry, Multidisciplinary

Continuous-flow photochemical carbene transfer reactions

Claire Empel et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Manipulation of gas-liquid-liquid systems in continuous flow microreactors for efficient reaction processes

Yanyan Liu et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Article Chemistry, Multidisciplinary

Continuous photocatalyzed aerobic oxidation of benzylic organotrifluoroborates to benzaldehydes under Taylor flow conditions

Melanie Roseau et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Scaling continuous API synthesis from milligram to kilogram: extending the enabling benefits of micro to the plant

Mateo Berton et al.

JOURNAL OF FLOW CHEMISTRY (2020)

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Review Chemistry, Multidisciplinary

Flow Photochemistry as a Tool in Organic Synthesis

Thomas H. Rehm

CHEMISTRY-A EUROPEAN JOURNAL (2020)

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Article Chemistry, Multidisciplinary

Discrete Ti-O-Ti Complexes: Visible-Light-Activated, Homogeneous Alternative to TiO2Photosensitisers

Kira Behm et al.

CHEMISTRY-A EUROPEAN JOURNAL (2020)

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Review Chemistry, Multidisciplinary

Catalytic Enantioselective Radical Transformations Enabled by Visible Light

Debajyoti Saha

CHEMISTRY-AN ASIAN JOURNAL (2020)

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Review Chemistry, Multidisciplinary

Continuous-flow photochemistry: An expanding horizon of sustainable technology

Jingli Xie et al.

CHINESE CHEMICAL LETTERS (2020)

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Article Chemistry, Physical

On factors limiting the performance of photoelectrochemical CO2 reduction

Ya Liu et al.

JOURNAL OF CHEMICAL PHYSICS (2020)

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Review Chemistry, Multidisciplinary

A review of enantioselective dual transition metal/photoredox catalysis

Hong-Hao Zhang et al.

SCIENCE CHINA-CHEMISTRY (2020)

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Article Chemistry, Medicinal

Current and Future Roles of Artificial Intelligence in Medicinal Chemistry Synthesis

Thomas J. Struble et al.

JOURNAL OF MEDICINAL CHEMISTRY (2020)

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Article Chemistry, Organic

Total Synthesis of (+)-Polyoxamic Acid via Visible-Light-Mediated Photocatalytic β-Scission and 1,5-Hydrogen Atom Transfer of Glucose Derivative

Takuro Matsuoka et al.

JOURNAL OF ORGANIC CHEMISTRY (2020)

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Article Chemistry, Physical

Visible light catalyzed anti-markovnikov hydration of styrene to 2-phenylethanol: From batch to continuous

Yuhang Chen et al.

JOURNAL OF PHOTOCHEMISTRY AND PHOTOBIOLOGY A-CHEMISTRY (2020)

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Article Chemistry, Multidisciplinary

Organophotoredox Hydrodefluorination of Trifluoromethylarenes with Translational Applicability to Drug Discovery

Jeroen B. Sap et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2020)

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Article Chemistry, Multidisciplinary

An Integrated Device for the Solar-Driven Electrochemical Conversion of CO2 to CO

Adriano Sacco et al.

ACS SUSTAINABLE CHEMISTRY & ENGINEERING (2020)

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Article Polymer Science

The Promising Future of Fluoropolymers

Bruno Ameduri

MACROMOLECULAR CHEMISTRY AND PHYSICS (2020)

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Review Chemistry, Physical

Recent Advances in Solar-Driven Carbon Dioxide Conversion: Expectations versus Reality

Jie He et al.

ACS ENERGY LETTERS (2020)

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Article Chemistry, Multidisciplinary

Light-Promoted Bromine-Radical-Mediated Selective Alkylation and Amination of Unactivated C(sp3)-H Bonds

Penghao Jia et al.

CHEM (2020)

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Article Multidisciplinary Sciences

Automated radial synthesis of organic molecules

Sourav Chatterjee et al.

NATURE (2020)

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Article Chemistry, Multidisciplinary

Scale-up Design of a Fluorescent Fluid Photochemical Microreactor by 3D Printing

Zhigang Zhu et al.

ACS OMEGA (2020)

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Review Chemistry, Multidisciplinary

The Concept of Chemical Generators: On-Site On-Demand Production of Hazardous Reagents in Continuous Flow

Doris Dallinger et al.

ACCOUNTS OF CHEMICAL RESEARCH (2020)

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Article Chemistry, Applied

Photo-oxidation of Cyclopentadiene Using Continuous Processing: Application to the Synthesis of (1R,4S)-4-Hydroxycyclopent-2-en-1-yl Acetate

Elena Herrero-Gomez et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2020)

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Decarboxylative Intramolecular Arene Alkylation Using N-(Acyloxy)phthalimides, an Organic Photocatalyst, and Visible Light

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Late-Stage 18F-Difluoromethyl Labeling of N-Heteroaromatics with High Molar Activity for PET Imaging

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Implementing Hydrogen Atom Transfer (HAT) Catalysis for Rapid and Selective Reductive Photoredox Transformations in Continuous Flow

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Visible-Light-Mediated lodoperfluoroalkylation of Alkenes in Flow and Its Application to the Synthesis of a Key Fulvestrant Intermediate

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Visible-Light-Mediated Cross-Couplings and C-H Activation via Dual Photoredox/Transition-Metal Catalysis in Continuous-Flow Processes

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Energy-Efficient Solar Photochemistry with Luminescent Solar Concentrator Based Photomicroreactors

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Accessing 1,2-Substituted Cyclobutanes through 1,2-Azaborine Photoisomerization

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被撤回的出版物: Reductive Arylation of Arylidene Malonates Using Photoredox Catalysis (Retracted Article)

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Finding the Perfect Match: A Combined Computational and Experimental Study toward Efficient and Scalable Photosensitized [2+2] Cycloadditions in Flow

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Catalytic Generation and Use of Ketyl Radical from Unactivated Aliphatic Carbonyl Compounds

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Continuous Flow Synthesis of Isoxazoles via Vinyl Azides from Friedel-Crafts Acylation of Alkynes: A Modulated Troubleshooting Optimization Approach

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A Laser Driven Flow Chemistry Platform for Scaling Photochemical Reactions with Visible Light

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Gas-Diffusion Electrodes for Carbon Dioxide Reduction: A New Paradigm

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High throughput analysis enables high throughput experimentation in pharmaceutical process research

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In-flow photooxygenation of aminothienopyridinones generates iminopyridinedione PTP4A3 phosphatase inhibitors

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Photochemical benzylic bromination in continuous flow using BrCCl3 and its application to telescoped p-methoxybenzyl protection

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Towards a Scalable Synthesis of 2-Oxabicyclo[2.2.0]hex-5-en-3-one Using Flow Photochemistry

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Integrated continuous flow/batch protocol for the photoreduction of ortho-methyl phenyl ketones using water as the hydrogen source

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Sensitized [2+2] intramolecular photocycloaddition of unsaturated enones using UV LEDs in a continuous flow reactor: kinetic and preparative aspects

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CO2, water, and sunlight to hydrocarbon fuels: a sustained sunlight to fuel (Joule-to-Joule) photoconversion efficiency of 1%

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Photoredox Ni-catalyzed peptide C(sp2)-O cross-coupling: from intermolecular reactions to side chain-to-tail macrocyclization

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Visible light-mediated photo-oxygenation of arylcyclohexenes

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Photoelectrochemical cell for P-H/C-H cross-coupling with hydrogen evolution

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Enantioselective photooxygenation of β-dicarbonyl compounds in batch and flow photomicroreactors

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Photochemical Flow Synthesis of 3-Hydroxyazetidines

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Cross coupling of alkylsilicates with acyl chlorides via photoredox/nickel dual catalysis: a new synthesis method for ketones

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Highly Performing Iodoperfluoroalkylation of Alkenes Triggered by the Photochemical Activity of Perylene Diimides

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Process Intensification for the Synthesis of 6-Allyl-6-azabicyclo[3.1.0]hex-3-en-2-ol from 1-Allylpyridinium Salt Using a Continuous UV-Light Photoflow Approach

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Photoelectrocatalytic arene C-H amination

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Visible-light-mediated deuteration of silanes with deuterium oxide

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Selective synthesis of azoxybenzenes from nitrobenzenes by visible light irradiation under continuous flow conditions

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Improved Reactor Productivity for the Safe Photo-Oxidation of Citronellol Under Visible Light LED Irradiation

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Mechanochemistry for Organic Chemists: An Update

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Acyl Radicals from Acylsilanes: Photoredox-Catalyzed Synthesis of Unsymmetrical Ketones

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Scale-up of a Luminescent Solar Concentrator-Based Photomicroreactor via Numbering-up

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Progress and Perspective of Electrocatalytic CO2 Reduction for Renewable Carbonaceous Fuels and Chemicals

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Electrolysis of Gaseous CO2 to CO in a Flow Cell with a Bipolar Membrane

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Eosin Y as a Direct Hydrogen-Atom Transfer Photocatalyst for the Functionalization of C-H Bonds

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A Fully Automated Continuous-Flow Platform for Fluorescence Quenching Studies and Stern-Volmer Analysis

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Continuous Visible-Light Photoflow Approach for a Manganese-Catalyzed (Het)Arene C-H Arylation

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The Dewar Isomer of 1,2-Dihydro-1,2-azaborinines: Isolation, Fragmentation, and Energy Storage

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Selective C(sp(3))-H Aerobic Oxidation Enabled by Decatungstate Photocatalysis in Flow

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Process Analysis on Preparation of Cyclobutanetetracarboxylic Dianhydride in a Photomicroreactor within Gas-Liquid Taylor Flow

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Photocatalytic carbon dioxide reduction to fuels in continuous flow monolith photoreactor using montmorillonite dispersed Fe/TiO2 nanocatalyst

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Continuous Endoperoxidation of Conjugated Dienes and Subsequent Rearrangements Leading to C-H Oxidized Synthons

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Sensitized Aliphatic Fluorination Directed by Terpenoidal Enones: A Visible Light Approach

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Generation of Diversity Sets with High sp3 Fraction Using the Photoredox Coupling of Organotrifluoroborates and Organosilicates with Heteroaryl/Aryl Bromides in Continuous Flow

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Visible-Light Photocatalytic Difluoroalkylation-Induced 1, 2-Heteroarene Migration of Allylic Alcohols in Batch and Flow

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Modulation of reactivity of singlet radical pair in continuous flow: Photo-Fries rearrangement

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Unexpected regioselectivity in the photocyclization of a chiral 2,3-bisbenzylidenesuccinate, leading to a podophyllotoxin related cyclolignan

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Transitioning from conventional batch to microfluidic processes for the efficient singlet oxygen photooxygenation of methionine

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Hot Hole Collection and Photoelectrochemical CO2 Reduction with Plasmonic Au/p-GaN Photocathodes

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Iridium-catalyzed Synthesis of Saturated N-Heterocycles from Aldehydes and SnAP Reagents with Continuous Flow Photochemistry

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Development of a Flow Photochemical Aerobic Oxidation of Benzylic C-H Bonds

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Electrochemical Formation of N-Acyloxy Amidyl Radicals and Their Application: Regioselective Intramolecular Amination of sp(2) and sp(3) C-H Bonds

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Flow Photochemistry as a Tool for the Total Synthesis of (+)-Epigalcatin

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Photocatalytic and Chemoselective Transfer Hydrogenation of Diarylimines in Batch and Continuous Flow

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Radical Carbonylation Mediated by Continuous-Flow Visible-Light Photocatalysis: Access to 2,3-Dihydrobenzofurans

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Microflow High-p,T Intensification of Vitamin D3 Synthesis Using an Ultraviolet Lamp

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Flow-Assisted Synthesis of Bicyclic Aziridines via Photochemical Transformation of Pyridinium Salts

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Photoredox Iridium Nickel Dual-Catalyzed Decarboxylative Arylation Cross-Coupling: From Batch to Continuous Flow via Self Optimizing Segmented Flow Reactor

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UV PhotoVap: Demonstrating How a Simple and Versatile Reactor Based on a Conventional Rotary Evaporator Can Be Used for UV Photochemistry

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Mapping the dark space of chemical reactions with extended nanomole synthesis and MALDI-TOF MS

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Combining C-H functionalisation and flow photochemical heterocyclic metamorphosis (FP-HM) for the synthesis of benzo[1,3]oxazepines

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Recyclable alkylated Ru(bpy)32+ complex as a visible-light photoredox catalyst for perfluoroalkylation

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Machine assisted reaction optimization: A self-optimizing reactor system for continuous-flow photochemical reactions

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Combining engineering and chemistry for the selective continuous production of four different oxygenated compounds by photo-oxidation of cyclopentadiene using liquid and supercritical CO2 as solvents

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Flow fine synthesis with heterogeneous catalysts

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Photochemical syntheses, transformations, and bioorthogonal chemistry of trans-cycloheptene and sila trans-cycloheptene Ag(I) complexes

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Radical-mediated direct C-H amination of arenes with secondary amines

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Artificial Photosynthesis for Formaldehyde Production with 85% of Faradaic Efficiency by Tuning the Reduction Potential

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Radical Fluoroalkylation Reactions

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Alkoxyl Radicals Generated under Photoredox Catalysis: A Strategy for anti-Markovnikov Alkoxylation Reactions

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Borocyclopropanation of Styrenes Mediated by UV-light Under Continuous Flow Conditions

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Microtubing-Reactor-Assisted Aliphatic C-H Functionalization with HCl as a Hydrogen-Atom-Transfer Catalyst Precursor in Conjunction with an Organic Photoredox Catalyst

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Redox-Active Reagents for Photocatalytic Generation of the OCF3 Radical and (Hetero)Aryl C-H Trifluoromethoxylation

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Photo-Electrochemical C-H Bond Activation of Cyclohexane Using a WO3 Photoanode and Visible Light

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Recent Advances in Photodecarboxylations Involving Phthalimides

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Light on the Horizon: Current Research and Future Perspectives in Flow Photochemistry

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Merging Transition-Metal Catalysis with Photoredox Catalysis: An Environmentally Friendly Strategy for C-H Functionalization

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Electrochemical-Oxidation-Induced Site-Selective Intramolecular C(sp(3))-H Amination

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Visible-Light-Mediated Metal-Free Difunctionalization of Alkenes with CO2 and Silanes or C(sp3)-H Alkanes

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Photochemical In-Flow Synthesis of 2,4-Methanopyrrolidines: Pyrrolidine Analogues with Improved Water Solubility and Reduced Lipophilicity

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Photochemical Homologation for the Preparation of Aliphatic Aldehydes in Flow

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Porphyrins as Photoredox Catalysts in Csp2-H Arylations: Batch and Continuous Flow Approaches

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Cerium-Catalyzed Formal Cycloaddition of Cycloalkanols with Alkenes through Dual Photoexcitation

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Three-Component Assembly of Multiply Substituted Homoallylic Alcohols and Amines Using a Flow Chemistry Photoreactor

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Scaling Up UV-Mediated Intramolecular Photodehydro-Diels-Alder Reactions Using a Homemade High-Performance Annular Continuous-Flow Reactor

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Photoelectrochemical Reactors for CO2 Utilization

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Liquid-Liquid Slug-Flow-Accelerated [2+2] Photocycloaddition of Cinnamates

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Exploiting Photochemical Processes in Multi-Step Continuous Flow: Derivatization of the Natural Product Clausine C

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Laser-Mediated Photo-High-p,T Intensification of Vitamin D3 Synthesis in Continuous Flow

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Multi-Step Continuous Flow Synthesis of /-Substituted Ketones

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Studies Toward the Scaling of Gas-Liquid Photocycloadditions

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Photoinduced Rearrangement of Dienones and Santonin Rerouted by Amines

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Advances in the Synthesis of Aryltetralin and Arylnaphthalene Lignans using Photocyclization

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Photochemically Produced Singlet Oxygen: Applications and Perspectives

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Alumina-Supported CoFe Alloy Catalysts Derived from Layered-Double-Hydroxide Nanosheets for Efficient Photothermal CO2 Hydrogenation to Hydrocarbons

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Recent Developments in the Photo-Mediated Generation of Silyl Radicals and Their Application in Organic Synthesis

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One-Pot Synthesis of Diverse -Lactam Scaffolds Facilitated by a Nebulizer-Based Continuous Flow Photoreactor

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Continuous Flow Photochemical Benzylic Bromination of a Key Intermediate in the Synthesis of a 2-Oxazolidinone

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Continuous Flow for the Photochemical C-H Amination of Arenes

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Rapid Production of trans-Cyclooctenes in Continuous Flow

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Acetic Acid Accelerated Visible-Light Photoredox Catalyzed N-Demethylation of N,N-Dimethylaminophenyl Derivatives

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Diverse Visible-Light-Promoted Functionalizations of Benzotriazoles Inspired by Mechanism-Based Luminescence Screening

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A Leaf-Inspired Luminescent Solar Concentrator for Energy-Efficient Continuous-Flow Photochemistry

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Improving the throughput of batch photochemical reactions using flow: Dual photoredox and nickel catalysis in flow for C(sp2)-C(sp3) cross-coupling

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Sunflow: Sunlight Drives Fast and Green Photochemical Flow Reactions in Simple Microcapillary Reactors - Application to Photoredox and H-Atom-Transfer Chemistry

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Photoredox activation of carbon dioxide for amino acid synthesis in continuous flow

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Cyclopropenium Salts as Cyclable, High-Potential Catholytes in Nonaqueous Media

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Targeting Activation of CO2 and H2 over Ru-Loaded Ultrathin Layered Double Hydroxides to Achieve Efficient Photothermal CO2 Methanation in Flow-Type System

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Mechanochemistry: A Force of Synthesis

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A prototype reactor for highly selective solar-driven CO2 reduction to synthesis gas using nanosized earth-abundant catalysts and silicon photovoltaics

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From millimetres to metres: the critical role of current density distributions in photo-electrochemical reactor design

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Hydrogen Atom Transfer (HAT): A Versatile Strategy for Substrate Activation in Photocatalyzed Organic Synthesis

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Photocatalysis in Organic Synthesis - Past, Present, and Future

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Scalable Flow Synthesis of [6,6]-Phenyl-C61-butyric Acid Methyl Ester (PCBM) using a Flow Photoreactor with a Sodium Lamp

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Syngas production from electrochemical reduction of CO2: current status and prospective implementation

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A laboratory-scale annular continuous flow reactor for UV photochemistry using excimer lamps for discrete wavelength excitation and its use in a wavelength study of a photodecarboxlyative cyclisation

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Photochemical intramolecular amination for the synthesis of heterocycles

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Visible-Light Driven Photocascade Catalysis: Union of N,N-Dimethylanilines and α-Azidochalcones in Flow Microreactors

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Formal Total Synthesis of L-Ossamine via Decarboxylative Functionalization Using Visible-Light-Mediated Photoredox Catalysis in a Flow System

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Approach to Comparing the Functional Group Tolerance of Reactions

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Total Synthesis of Zaragozic Acid C: Implementation of Photochemical C(sp3)-H Acylation

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Photoinduced Nickel-Catalyzed Chemo- and Regioselective Hydroalkylation of Internal Alkynes with Ether and Amide α-Hetero C(sp3)-H Bonds

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Chemo- and Regioselective Organo-Photoredox Catalyzed Hydroformylation of Styrenes via a Radical Pathway

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18F-Fluorination of Unactivated C-H Bonds in Branched Aliphatic Amino Acids: Direct Synthesis of Oncological Positron Emission Tomography Imaging Agents

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Multiple Enone-Directed Reactivity Modes Lead to the Selective Photochemical Fluorination of Polycyclic Terpenoid Derivatives

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Direct β-Selective Hydrocarboxylation of Styrenes with CO2 Enabled by Continuous Flow Photoredox Catalysis

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Predictive Model for Site-Selective Aryl and Heteroaryl C-H Functionalization via Organic Photoredox Catalysis

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Blue-light-promoted carbon-carbon double bond isomerization and its application in the syntheses of quinolines

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Synthesis of cyclopent-2-enones from furans using a nebulizer-based continuous flow photoreactor

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A photoredox-neutral Smiles rearrangement of 2-aryloxybenzoic acids

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Continuous Flow α-Arylation of N,N-Dialkylhydrazones under Visible-Light Photoredox Catalysis

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ORGANIC LETTERS (2017)

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Continuous Flow Synthesis of Morpholines and Oxazepanes with Silicon Amine Protocol (SLAP) Reagents and Lewis Acid Facilitated Photoredox Catalysis

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Continuous Photo-Oxidation in a Vortex Reactor: Efficient Operations Using Air Drawn from the Laboratory

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Continuous-Flow Preparation of γ-Butyrolactone Scaffolds from Renewable Fumaric and Itaconic Acids under Photosensitized Conditions

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Scalable Photocatalytic Oxidation of Methionine under Continuous-Flow Conditions

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Automated glycan assembly using the Glyconeer 2.1 synthesizer

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Convenient Phenacene Synthesis by Sequentially Performed Wittig Reaction and Mallory Photocyclization Using Continuous-Flow Techniques

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Visible-Light-Induced Trifluoromethylation of Highly Functionalized Arenes and Heteroarenes in Continuous Flow

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Design and Scaling Up of Microchemical Systems: A Review

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ANNUAL REVIEW OF CHEMICAL AND BIOMOLECULAR ENGINEERING, VOL 8 (2017)

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Direct Cα-heteroarylation of structurally diverse ethers via a mild N-hydroxysuccinimide mediated cross-dehydrogenative coupling reaction

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Metal-free direct alkylation of unfunctionalized allylic/benzylic sp3 C-H bonds via photoredox induced radical cation deprotonation

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Reaction discovery using acetylene gas as the chemical feedstock accelerated by the stop-flow micro-tubing reactor system

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Micro-flow photosynthesis of new dienophiles for inverse-electron-demand Diels-Alder reactions. Potential applications for pretargeted in vivo PET imaging

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Photoelectrochemical oxidation of organic substrates in organic media

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Regioselective Synthesis of 2-Substituted indoles from Benzotriazoles and Alkynes by Photoinitiated Denitrogenation

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Polymer-Supported Photosensitizers for Oxidative Organic Transformations in Flow and under Visible Light Irradiation

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Visible-Light-Mediated Anti-Markovnikov Hydration of Olefins

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Visible-Light Photocatalytic Decarboxylation of α,β-Unsaturated Carboxylic Acids: Facile Access to Stereoselective Difluoromethylated Styrenes in Batch and Flow

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Merger of Visible-Light Photoredox Catalysis and C-H Activation for the Room-Temperature C-2 Acylation of lndoles in Batch and Flow

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Rapid and facile chemical actinometric protocol for photo-microfluidic systems using azobenzene and NMR spectroscopy

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RSC ADVANCES (2017)

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A Personal Perspective on the Future of Flow Photochemistry

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Metal-Free [2+2]-Photocycloaddition of (Z)-4-Aryliden-5(4H)-Oxazolones as Straightforward Synthesis of 1,3-Diaminotruxillic Acid Precursors: Synthetic Scope and Mechanistic Studies

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An In-Depth Study of the Use of Eosin Y for the Solar Photocatalytic Oxidative Coupling of Benzylic Amines

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Toward a Practical Solar-Driven CO2 Flow Cell Electrolyzer: Design and Optimization

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Triphenothiazinyl triazacoronenes: donor-acceptor molecular graphene exhibiting multiple fluorescence and electrogenerated chemiluminescence emissions

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JOURNAL OF MATERIALS CHEMISTRY C (2017)

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Photoelectrochemical Oxidation of Benzylic Alcohol Derivatives on BiVO4/WO3 under Visible Light Irradiation

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CHEMELECTROCHEM (2017)

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Redox Catalysis Facilitates Lignin Depolymerization

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A General Small-Scale Reactor To Enable Standardization and Acceleration of Photocatalytic Reactions

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ACS CENTRAL SCIENCE (2017)

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Assessing inter- and intramolecular continuous-flow strategies towards methylphenidate (Ritalin) hydrochloride

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Solvent-free coupling of aryl halides with pyrroles applying visible-light photocatalysis

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Singlet oxygen oxidations in homogeneous continuous flow using a gas-liquid membrane reactor

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Every photon counts: understanding and optimizing photon paths in luminescent solar concentrator-based photomicroreactors (LSC-PMs)

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Continuous-flow synthesis of fluorine-containing fine chemicals with integrated benchtop NMR analysis

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Safety assessment in development and operation of modular continuous-flow processes

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The merger of transition metal and photocatalysis

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The photodecarboxylative addition of carboxylates to phthalimides as a key-step in the synthesis of biologically active 3-arylmethylene-2,3-dihydro-1H-isoindolin-1-ones

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BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY (2017)

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Heuristics, Protocol, and Considerations for Flow Chemistry in Photoredox Catalysis

Eric G. Moschetta et al.

CHEMPHOTOCHEM (2017)

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High lumen density sources based on LED-pumped phosphor rods: opportunities for performance improvement

Dick K. G. de Boer et al.

SIXTEENTH INTERNATIONAL CONFERENCE ON SOLID STATE LIGHTING AND LED-BASED ILLUMINATION SYSTEMS (2017)

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A Versatile Route to Unstable Diazo Compounds via Oxadiazolines and their Use in Aryl-Alkyl Cross-Coupling Reactions

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2017)

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Visible-Light-Mediated Metal-Free Hydrosilylation of Alkenes through Selective Hydrogen Atom Transfer for Si-H Activation

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2017)

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High throughput photo-oxidations in a packed bed reactor system

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Photosynthesis of formate from CO2 and water at 1% energy efficiency via copper iron oxide catalysis

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Experimental demonstrations of spontaneous, solar-driven photoelectrochemical water splitting

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Unexpected Dual Role of Titanium Dioxide in the Visible Light Heterogeneous Catalyzed C-H Arylation of Heteroarenes

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Optimal ways of colour mixing for high-quality white-light LED sources

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Rapid Trifluoromethylation and Perfluoroalkylation of Five-Membered Heterocycles by Photoredox Catalysis in Continuous Flow

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Direct C-N Coupling of Imidazoles with Aromatic and Benzylic Compounds via Electrooxidative C-H Functionalization

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A novel photoelectrochemical flow cell with online mass spectrometric detection: oxidation of formic acid on a nanocrystalline TiO2 electrode

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CO2 Reduction to Methanol on TiO2-Passivated GaP Photocatalysts

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A versatile photoanode-driven photoelectrochemical system for conversion of CO2 to fuels with high faradaic efficiencies at low bias potentials

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Efficient solar photoelectrosynthesis of methanol from carbon dioxide using hybrid CuO-Cu2O semiconductor nanorod arrays

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Photoremovable Protecting Groups in Chemistry and Biology: Reaction Mechanisms and Efficacy

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Tailoring Copper Oxide Semiconductor Nanorod Arrays for Photoelectrochemical Reduction of Carbon Dioxide to Methanol

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Oxazolone-Based Photoswitches: Synthesis and Properties

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Visible Light Driven Water Splitting in a Molecular Device with Unprecedentedly High Photocurrent Density

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Electrochemical C-H Amination: Synthesis of Aromatic Primary Amines via N-Arylpyridinium Ions

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PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA (2013)

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Strategic Redox Relay Enables A Scalable Synthesis of Ouabagenin, A Bioactive Cardenolide

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Allylic Oxidations of Olefins to Enones

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Through-Wall Mass Transport as a Modality for Safe Generation of Singlet Oxygen in Continuous Flows

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Unexpected N-Demethylation of Oxymorphone and Oxycodone N-Oxides Mediated by the Burgess Reagent: Direct Synthesis of Naltrexone, Naloxone, and Other Antagonists from Oxymorphone

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Continuous-Flow Synthesis of the Anti-Malaria Drug Artemisinin

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Photochemical and Photoelectrochemical Reduction of CO2

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ANNUAL REVIEW OF PHYSICAL CHEMISTRY, VOL 63 (2012)

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Novel potent dual inhibitors of CK2 and Pim kinases with antiproliferative activity against cancer cells

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Cyclobutane Derivatives As Novel Nonpeptidic Small Molecule Agonists of Glucagon-Like Peptide-1 Receptor

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Functionally Diverse Nucleophilic Trapping of Iminium Intermediates Generated Utilizing Visible Light

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Catalyst and solvent-free bromination of toluene derivatives by HBr-H2O2 with visible-light photocatalysis using a continuous-flow micro reactor

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Visible light-induced partial oxidation of cyclohexane on WO3 loaded with Pt nanoparticles

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Photochemical Reactions as Key Steps in Natural Product Synthesis

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Triple-channel microreactor for biphasic gas-liquid reactions: Photosensitized oxygenations

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A visible light water-splitting cell with a photoanode formed by codeposition of a high-potential porphyrin and an iridium water-oxidation catalyst

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Chiral Sulfoxides as Metabolites of 2-Thioimidazole-Based p38α Mitogen-Activated Protein Kinase Inhibitors: Enantioselective Synthesis and Biological Evaluation

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Design, Synthesis, and X-ray Crystallographic Analysis of a Novel Class of HIV-1 Protease Inhibitors

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Continuous Flow Synthesis of Fullerene Derivatives

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A Versatile and Stereoselective Synthesis of Functionalized Cyclobutenes

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Technology development for the production of biobased products from biorefinery carbohydrates-the US Department of Energy's Top 10 revisited

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Solar Driven Water Oxidation by a Bioinspired Manganese Molecular Catalyst

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Photodimerization of Maleic Anhydride in a Microreactor Without Clogging

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Overcoming the Challenges of Solid Bridging and Constriction during Pd-Catalyzed C-N Bond Formation in Microreactors

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Unexpected [2+2] C-C bond coupling due to photocycloaddition on orthopalladated (Z)-2-aryl-4-arylidene-5(4H)-oxazolones

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Photoinduced activation of CO2 on Ti-based heterogeneous catalysts: Current state, chemical physics-based insights and outlook

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Structure, Energy, Synergy, Time-The Fundamentals of Process Intensification

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Photoassisted Overall Water Splitting in a Visible Light-Absorbing Dye-Sensitized Photoelectrochemical Cell

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α-Haloarylsulfonamides: multiple cyclization pathways to skeletally diverse benzofused sultams

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Thiourea-enhanced flavin photooxidation of benzyl alcohol

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Gas-Liquid Microreaction Technology: Recent Developments and Future Challenges

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A photochemical synthesis of functionalized trans-cyclooctenes driven by metal complexation

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Ultraviolet light-emitting diodes based on group three nitrides

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Experimental and numerical model study of the limiting current in a channel flow cell with a circular electrode

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2008)

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Article Energy & Fuels

A review of intensification of photocatalytic processes

Tom Van Gerven et al.

CHEMICAL ENGINEERING AND PROCESSING-PROCESS INTENSIFICATION (2007)

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Article Polymer Science

Performance of the light emitting diodes versus conventional light sources in the UV light cured formulations

Kelechi C. Anyaogu et al.

JOURNAL OF APPLIED POLYMER SCIENCE (2007)

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Review Electrochemistry

Hydrogen generation at irradiated oxide semiconductor-solution interfaces

Krishnan Rajeshwar

JOURNAL OF APPLIED ELECTROCHEMISTRY (2007)

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Review Chemistry, Multidisciplinary

Recent developments in the synthesis of prostaglandins and analogues

Saibal Das et al.

CHEMICAL REVIEWS (2007)

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Review Chemistry, Multidisciplinary

Photocatalysis for the formation of the C-C bond

Maurizio Fagnoni et al.

CHEMICAL REVIEWS (2007)

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Correction Biochemical Research Methods

Multiphase microfluidics: from flow characteristics to chemical and materials synthesis (vol 6, pg 1487, 2006)

Axel Guenther et al.

LAB ON A CHIP (2007)

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Correction Biochemical Research Methods

Multiphase microfluidics: from flow characteristics to chemical and materials synthesis (vol 6, pg 1487, 2006)

Axel Gunther et al.

LAB ON A CHIP (2007)

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Review Biochemical Research Methods

Multiphase microfluidics:: from flow characteristics to chemical and materials synthesis

Axel Gunther et al.

LAB ON A CHIP (2006)

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Article Chemistry, Applied

Experiences with commercial production scale operation of dissolving metal reduction using lithium metal and liquid ammonia

DK Joshi et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2005)

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Article Chemistry, Organic

A practical flow reactor for continuous organic photochemistry

BDA Hook et al.

JOURNAL OF ORGANIC CHEMISTRY (2005)

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Article Chemistry, Physical

Electrochemical mass spectroscopic and surface photovoltage studies of catalytic water photooxidation by undoped and carbon-doped titania

B Neumann et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2005)

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Article Engineering, Chemical

Carbon dioxide absorption in a falling film microstructured reactor: Experiments and modeling

M Zanfir et al.

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH (2005)

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Review Chemistry, Multidisciplinary

Selectfluor: Mechanistic insight and applications

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2005)

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Article Chemistry, Multidisciplinary

Electroorganic synthesis on the solid phase using polymer beads as supports

S Nad et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2004)

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Green chemistry and photochemistry were born at the same time

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GREEN CHEMISTRY (2004)

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Review Chemistry, Multidisciplinary

Protection (and deprotection) of functional groups in organic synthesis by heterogeneous catalysis

G Sartori et al.

CHEMICAL REVIEWS (2004)

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Article Chemistry, Applied

Catalyst preparation and deactivation issues for nitrobenzene hydrogenation in a microstructured falling film reactor

KK Yeong et al.

CATALYSIS TODAY (2003)

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Article Chemistry, Organic

The mechanism of the tertiary amine catalysed isomerisation of endoperoxides to hydroxyketones: synthesis and chemistry of the intermediate postulated in the peroxide attack mechanism

DR Kelly et al.

TETRAHEDRON LETTERS (2002)

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Article Chemistry, Applied

A microfabricated nanoreactor for safe, continuous generation and use of singlet oxygen

RCR Wootton et al.

ORGANIC PROCESS RESEARCH & DEVELOPMENT (2002)

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Photoelectrochemical cells

M Grätzel

NATURE (2001)

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Article Chemistry, Physical

Factors affecting the rate of decay of the first excited singlet state of molecular oxygen O2(a1Δg) in supercritical fluid carbon dioxide

DR Worrall et al.

JOURNAL OF PHYSICAL CHEMISTRY A (2001)

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Review Chemistry, Multidisciplinary

Experimental strategies for combinatorial and high-throughput materials development

JN Cawse

ACCOUNTS OF CHEMICAL RESEARCH (2001)

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Article Chemistry, Medicinal

2-carbomethoxy-3-aryl-8-bicyclo[3.2.1]octanes: Potent non-nitrogen inhibitors of monoamine transporters

PC Meltzer et al.

JOURNAL OF MEDICINAL CHEMISTRY (2000)

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