4.7 Article

Fused deposition fabrication of high-quality zirconia ceramics using granular feedstock

Journal

CERAMICS INTERNATIONAL
Volume 47, Issue 24, Pages 34352-34360

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.08.348

Keywords

Fused deposition modeling; Additive manufacturing; 3D ceramics; Printing steps; Thermal accumulation

Funding

  1. National Natural Science Foundation of China [52074365]
  2. Hunan Province, China [2020JJ4731]
  3. State Key Laboratory of Powder Metallurgy, Central South University, Changsha, China

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This study fabricated 3D zirconia ceramics using granular feedstock and analyzed their morphology, surface quality, and the effect of thermal accumulation on structure. The research showed that small printing size increased thermal accumulation and decreased printing quality.
Benefiting from the mature technology of ceramic injection molding, Fused deposition modeling based on highly-filled ceramic-polymer granular feedstocks has been showing great potential and advantage for fabricating 3D ceramics. Herein, 3D zirconia ceramics using granular feedstock were fabricated, and typical morphology, sur -face quality, and effect of the thermal accumulation on 3D structure were clarified. Typical morphology of printing steps on the surface were quantitatively characterized, and determined by the surface curvature and layer height of the printed structure. Aligned triangular pores were confirmed at the junction of the deposited filaments with elliptical cross-section morphology. Simple square plates with different size were used to illustrate the influence of thermal accumulation on the morphology of 3D structure. Small printing size increased the thermal accumulation during deposition, resulting in decreased printing quality caused by the secondary over-melting of former deposited layers. Except for the pores at the junctions, dense zirconia ceramics with uni-form structure and smooth surface could be achieved. A low-cost and high-quality route for the preparation of 3D ceramics was demonstrated via FDM of highly-filled granular feedstocks.

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