4.7 Article

Nano-scale mechanical behaviors and material removal mechanisms of zirconia ceramics sintered at various temperatures

Journal

CERAMICS INTERNATIONAL
Volume 47, Issue 23, Pages 32588-32598

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.08.154

Keywords

Sintering process; Nanoindentation; Nanoscratch; Mechanical properties; Material removal mechanisms

Funding

  1. National Natural Science Foundation of China [52175425]

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The study found that 1100 degrees C is the transition threshold for the ceramic microstructure and mechanical properties, as well as for the transition in material removal mechanism from plastic regime to ductile-brittle characteristics.
The present work aims to address the effects of the sintering temperature (800-1500 degrees C) on the mechanical properties and material removal mechanisms of 3 mol% yttria-stabilized tetragonal zirconia polycrystals (3YTZP) based on a series of nanoindentation and nanoscratch experiments. The impacts of the sintering temperature on the mechanical properties, including plasticity, deformation behavior, indentation energies, and cracking resistance were rigorously studied. The acquired results indicate that 1100 degrees C signifies the transition threshold for the ceramic microstructure, leading to the entirely different mechanical properties and indentation responses for materials sintered at temperatures lower or higher than the threshold value. Moreover, 1100 degrees C is also a transition threshold of the material removal mechanism, before which the material removal mechanism is dominated by the plastic regime, and beyond which, the material removal mechanism tends to show ductilebrittle characteristics.

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