Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 363, Issue 13, Pages 3240-3244Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.202100228
Keywords
1,3-Diketones; Potassium thiocyanate; Thiazol-2(311)-ones; Transition-metal-free; Cyclization
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Funding
- National Natural Science Foundation of China [21672086]
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A strategy promoted by I-2 has been developed for the synthesis of thiazol-2(3H)-one derivatives, involving C-S and C-N bond formation with good functional group tolerance. A series of thiazol-2(3H)-one derivatives are obtained in moderate to good yields.
An I-2 -promoted strategy has been developed for the synthesis of thiazol-2(3H)-one derivatives from 1,3-diketones with potassium thiocyanate. This [3 + 2] cyclization reaction involves C-S and C-N bond formation and exhibits good functional group tolerance. A series of thiazol-2(3H)-one derivatives are obtained in moderate to good yields.
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