4.6 Article

Preparation and Electron-Beam Surface Modification of Novel TiNi Material for Medical Applications

Journal

APPLIED SCIENCES-BASEL
Volume 11, Issue 10, Pages -

Publisher

MDPI
DOI: 10.3390/app11104372

Keywords

TiNi; high-current pulsed electron beam; porous coating; surface modification; EIS in saline; cell growth

Funding

  1. Russian Science Foundation [19-79-10045]
  2. Russian Science Foundation [19-79-10045] Funding Source: Russian Science Foundation

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The study focused on developing new materials and coatings for medical applications, utilizing a novel approach to fabricate TiNi surfaces and investigating structural and compositional changes caused by high-current-pulsed electron beam treatment. Additionally, the study examined the surface properties of the samples during storage in saline and conducted a model experiment with cell growth to evaluate cell appearance on different surface locations.
Featured Application Materials and coatings for medical applications. A new approach to fabricate TiNi surfaces combining the advantages of both monolithic and porous materials for implants is used in this work. New materials were obtained by depositing a porous TiNi powder onto monolithic TiNi plates followed by sintering at 1200 degrees C. Then, further modification of the material surface with a high-current-pulsed electron beam (HCPEB) was carried out. Three materials obtained (one after sintering and two after subsequent beam treatment by 30 pulses with different pulse energy) were studied by XRD, SEM, EDX, surface profilometry, and by means of electrochemical measurements, including OCP and EIS. Structural and compositional changes caused by HCPEB treatment were investigated. Surface properties of the samples during their storage in saline for 10 days were studied and a model experiment with cell growth (MCF-7) was carried out for the unmodified sample with an electron beam to detect cell appearance on different surface locations.

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