Journal
MATERIALS
Volume 14, Issue 9, Pages -Publisher
MDPI
DOI: 10.3390/ma14092148
Keywords
coordination compound; copper; tiglic acid; crystal structure; IR spectroscopy; thermal analysis; magnetic properties
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Funding
- Ministry of Science and Higher Education (Poland) [SPUB/SP/457471/2020]
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This study synthesized and crystallized a new coordination compound of copper and tiglic acid, named tetrakis(mu-tiglato)bis(tiglic acid)dicopper(II), and analyzed its structure and intermolecular interactions using X-ray diffraction measurement and Hirshfeld analysis. The compound was also characterized in terms of infrared absorption, thermal, and magnetic properties, revealing antiferromagnetic coupling of copper ions.
The first coordination compound of copper and tiglic acid named tetrakis(mu-tiglato)bis(tiglic acid)dicopper(II) was synthesized and crystallized from water solution. Its structure was determined and analyzed based on X-ray diffraction measurement. The paddle-wheel coordination system of the investigated compound was compared with other similar copper structures known in the literature. The Hirshfeld analysis was used for the detailed analysis of intermolecular interaction. The new compound was also characterized in terms of infrared absorption, thermal, and magnetic properties. The antiferromagnetic coupling of copper ions was found.
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