4.4 Article

Operando Neutron Scattering: Following Reactions in Real Time Using Neutrons

Journal

TOPICS IN CATALYSIS
Volume 64, Issue 9-12, Pages 693-698

Publisher

SPRINGER/PLENUM PUBLISHERS
DOI: 10.1007/s11244-021-01436-x

Keywords

Operando; Catalysis; Neutron diffraction; Quasielastic neutron scattering; QENS

Funding

  1. Science and Technology Facilities Council

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The article introduces the method of using neutron probes to observe the progress of catalytic reactions and the recent progress and possibilities in realistic applications.
The complexation of NiCl2 with 2,2 '-Bipyridine was followed using quasielastic neutron scattering to observe reaction progress. Water adsorption in chabazite with time resolution was observed using strain induced in the aluminosilicate framework with a high-resolution engineering diffractometer. These reactions illustrate the recent progress and possibilities in using neutron probes to observe realistic catalytic reactions as they progress.

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