4.7 Article

Sodium silicate effect on setting properties, strength behavior and microstructure of cemented coal fly ash backfill

Journal

POWDER TECHNOLOGY
Volume 384, Issue -, Pages 17-28

Publisher

ELSEVIER
DOI: 10.1016/j.powtec.2021.02.013

Keywords

Fly ash; Sodium silicate; Setting time; Coal mine; Compressive strength; Microstructure

Funding

  1. Karadeniz Technical University (KTU)
  2. Turkish Cement Manufacturers' Association (TCMB)

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This study investigated the effect of sodium silicate on early mechanical and microstructure properties of cemented coal fly ash backfill. Results showed that sodium silicate can improve the short-term strength of CCB and reduce the setting time, contributing to efficiency in coal mining operations.
Representing an engineered mixture of coal fly ash, cement and water, cemented coal fly ash backfill (CCB) is typically employed for filling the openings created after coal excavation in the earth. A high rate of productivity for coal mines requires a high early-age strength backfill design. Therefore, the use of admixtures in CCB is key for accelerating the backfill setting time and augmenting short-and long-term strength. This study offers the effect of sodium silicate (SS) as an accelerator on early age mechanical and microstructure properties of CCB. SSbased admixture was used for a dosage of 0.5,1 and 1.5 wt% in CCB that contains 25 wt% ordinary Portland cement OPC and 75 wt% coal fly ash. Backfill setting time was done by using the Vicat system while its strength and pore structure were measured by using the uniaxial compressive strength test, and scanning electron microscopy and Hg intrusion porosimetry. Results display that use of SS in CCB increases its short-term strength gain up to 14% and shortens the mining cycle by cutting its setting time up to 58%. The microstructure analyses also indicate that CCB formulated with SS has a finer pore structure than that without admixture. The outcomes of the present study will be advantageous to evaluate both setting time and strength behavior of CCB used in coal mines, thereby causing the effective backfill plan in terms of money saving and easy operation. Representing an engineered mixture of coal fly ash, cement and water, cemented coal fly ash backfill (CCB) is typically employed for filling the openings created after coal excavation in the earth. A high rate of productivity for coal mines requires a high early-age strength backfill design. Therefore, the use of admixtures in CCB is key for accelerating the backfill setting time and augmenting short-and long-term strength. This study offers the effect of sodium silicate (SS) as an accelerator on early age mechanical and microstructure properties of CCB. SS based admixture was used for a dosage of 0.5,1 and 1.5 wt% in CCB that contains 25 wt% ordinary Portland cement OPC and 75 wt% coal fly ash. Backfill setting time was done by using the Vicat system while its strength and pore structure were measured by using the uniaxial compressive strength test, and scanning electron microscopy and Hg intrusion porosimetry. Results display that use of SS in CCB increases its short-term strength gain up to 14% and shortens the mining cycle by cutting its setting time up to 58%. The microstructure analyses also indicate that CCB formulated with SS has a finer pore structure than that without admixture. The outcomes of the present study will be advantageous to evaluate both setting time and strength behavior of CCB used in coal mines, thereby causing the effective backfill plan in terms of money saving and easy operation. (c) 2021 Elsevier B.V. All rights reserved.

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