Journal
ORGANIC LETTERS
Volume 23, Issue 9, Pages 3772-3776Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.1c01184
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Funding
- National Natural Science Foundation of China [21871228, 22061044]
- Program for Changjiang Scholars and Innovative Research Team in University [IRT_17R94]
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An acylation reaction of arenes with aldehydes through dual CH activations at room temperature was reported. The reaction was initiated by phenanthraquinone-catalyzed hydrogen atom transfer from aldehyde under visible light irradiation, followed by the merging of the aldehyde-derived acyl radical with palladium-catalyzed activation of arenes to afford the cross coupling products.
An acylation of arenes with aldehydes through dual CH activations at room temperature is reported. The acylation was initiated by phenanthraquinone-catalyzed hydrogen atom transfer from aldehyde under visible light irradiation. The aldehyde-derived acyl radical merged with palladium-catalyzed activation of arenes to afford the cross coupling products.
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