Journal
JOURNAL OF MATERIALS SCIENCE
Volume 56, Issue 19, Pages 11494-11510Publisher
SPRINGER
DOI: 10.1007/s10853-021-06002-0
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Funding
- FAPESP (Sao Paulo Research Foundation) [2014/24449-0]
- CNPq (Brazilian National Council for Scientific and Technological Development) [155650/2018-1]
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Among the investigated beta-metastable alloys in the Ti-Nb-Fe-Zr system for biomedical applications, the addition of Fe as a minor alloying element has been explored to improve mechanical properties. The results show that Ti-23Nb-2.0Fe-10Zr alloy stands out with the best combination of mechanical strength and elastic modulus after aging, indicating great potential for biomedical applications.
Among many beta-metastable alloys explored for biomedical applications, alloys from the Ti-Nb-Fe-Zr system present great potential regarding cost and mechanical strength. In this article, we take a new look at the possibility of using Fe as a minor alloying element in the Ti-Nb-Fe-Zr system, with additions up to 2.0 wt% Fe. Additional compositions fixing the Nb/Fe ratio and changing Zr content from 7-13 wt% were also explored, resulting in a total of five different alloys. The samples were solution-treated and then subjected to three different conditions: water-quenched, furnace-cooled, and step-quenched to 450 degrees C for 12 h. Resultant microstructures were analyzed using X-ray diffraction, differential scanning calorimetry, scanning, and transmission electron microscopy. DSC experiments indicate that Zr might alter the phase transformations that occur during heating and cooling cycles. First-principles calculations confirmed that Zr's addition is crucial to reduce the elastic modulus of the beta matrix and increase the omega-phase formation energy relative to beta. All alloys presented mechanical properties suitable for biomedical applications; however, Ti-23Nb-2.0Fe-10Zr (wt %) stands out with the best combination of mechanical strength and elastic modulus after aging. [GRAPHICS] .
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