Journal
FOOD AND CHEMICAL TOXICOLOGY
Volume 151, Issue -, Pages -Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.fct.2021.112099
Keywords
NiFe nanoparticles; Polyaniline; Glucose; Non-enzymatic sensor; Selectivity; Reliability
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This article focuses on the fabrication of NiFe-Polyaniline glucose sensors via electrochemical technique. The fabricated sensor exhibited remarkable performance in terms of response time, sensitivity, and detection limit. The NiFe-PANi hybrid electrode shows promising potential for applications in electrochemical glucose sensing.
This article was focused on the elaboration of NiFe-Polyaniline glucose sensors via electrochemical technique. Firstly, the PANi (polyaniline) fibers were synthesized by oxidation of the monomer aniline on FTO (fluorine tin oxide) substrate. Secondly, the Nickel-Iron nanoparticles (NiFe (NPs)) were obtained by the Chronoamperometry method on the Polyaniline surface. The NiFe-PANi hybrid electrode was characterized by scanning electron microscopy (SEM), force atomic microscopy (AFM), Fourier-transformed infrared (FTIR), and X-ray diffraction (XRD). The electrochemical glucose sensing performance of the NiFe alloy nanoparticle was studied by cyclic voltammetry and amperometry. The fabricated glucose sensor Ni-Fe hybrid material exhibited many remarkable sensing performances, such as low-response time (4 s), sensitivity (1050 mu A mM(-1) cm(-2)), broad linear range (from 10 mu M - 1 mM), and low limit of detection (LOD) (0.5 mu M, S/N = 3). The selectivity, reliability, and stability of the NiFe hybrid material for glucose oxidation were also investigated. All the results demonstrated that the NiFe-PANi/FTO hybrid electrode is very promising for application in electrochemical glucose sensing.
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