Journal
ANNUAL REVIEW OF ANALYTICAL CHEMISTRY, VOL 14, 2021
Volume 14, Issue -, Pages 87-107Publisher
ANNUAL REVIEWS
DOI: 10.1146/annurev-anchem-091020-100631
Keywords
electrochemistry; surface X-ray diffraction; X-ray absorption; spectroscopy
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This article reviews the progress in material studies using X-ray techniques from an electrochemistry perspective, focusing on in situ/in operando surface X-ray scattering, X-ray absorption spectroscopy, and the combination of both methods. Key examples of in situ and in operando investigation of liquid-solid and liquid-liquid interfaces are presented. The article highlights the importance of X-ray scattering and spectroscopy in understanding electrocatalysis, electrodeposition, and battery materials, and discusses recent developments in the field.
This article reviews progress in the study of materials using X-ray-based techniques from an electrochemistry perspective. We focus on in situ/in operando surface X-ray scattering, X-ray absorption spectroscopy, and the combination of both methods. The background of these techniques together with key concepts is introduced. Key examples of in situ and in operando investigation of liquid-solid and liquid-liquid interfaces are presented. X-ray scattering and spectroscopy have helped to develop an understanding of the underlying atomic and molecular processes associated with electrocatalysis, electrodeposition, and battery materials. We highlight recent developments, including resonant surface diffraction and time-resolved studies.
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