Journal
SUSTAINABILITY
Volume 13, Issue 4, Pages -Publisher
MDPI
DOI: 10.3390/su13041788
Keywords
graphene nanoplatelets; graphene nanoplatelets; epoxy nanocomposite; mechanical properties; planetary centrifugal mixing; three-roll milling; traditional dispersal
Funding
- Ministry of Science and Technology (MOST) of Taiwan [MOST 107-2221-E-167-030-MY2]
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This study utilized planetary centrifugal mixing and three-roll milling as efficient dispersion methods to uniformly disperse graphene nanoplatelets in an epoxy solution, resulting in the preparation of graphene nanoplatelets/epoxy nanocomposites. The measurements of mechanical properties showed that planetary centrifugal mixing required shorter processing time and achieved a more uniform dispersion compared to three-roll milling, making it a more efficient dispersal method for epoxy-based nanocomposites preparation.
The preparation of polymer-based nanocomposites requires considerable time (i.e., the dispersal of nanomaterials into a polymer matrix), resulting in difficulties associated with their commercial use. In this study, two simple and efficient dispersion methods, namely planetary centrifugal mixing and three-roll milling, were used to enable the graphene nanoplatelets to disperse uniformly throughout an epoxy solution (i.e., 0, 0.1, 0.25, 0.5, and 1.0 wt.%) and allow the subsequent preparation of graphene nanoplatelets/epoxy nanocomposites. Measurements of mechanical properties of these nanocomposites, including ultimate tensile strength, flexural strength, and flexural modulus, were used to evaluate these dispersal methods. Dispersing graphene nanoplatelets into the epoxy resin by planetary centrifugal mixing not only required a shorter process time but also resulted in a more uniform dispersion of graphene nanoplatelets than that by three-roll milling. In addition, compared with traditional dispersal methods, planetary centrifugal mixing was a more efficient dispersal method for the preparation of epoxy-based nanocomposites.
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