4.7 Article

Microscale vacuum distillation apparatus for high-boiling, air- and heat-sensitive liquids

Journal

TALANTA
Volume 223, Issue -, Pages -

Publisher

ELSEVIER
DOI: 10.1016/j.talanta.2020.121747

Keywords

Microscale purification; Vacuum distillation; Air sensitive liquid

Funding

  1. National Science Foundation [CHE 1954745]

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The apparatus described enables vacuum distillation of 0.2 mL of air and water-sensitive, high boiling liquids, making it useful for teaching laboratories and practicing chemists.
We describe a simple apparatus that enables the vacuum distillation of-0.2 mL of airand water-sensitive, high boiling liquids. The apparatus should be useful in teaching laboratories, and also to practicing chemists.

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