Journal
ORGANIC LETTERS
Volume 23, Issue 4, Pages 1239-1242Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c04192
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Funding
- National Natural Science Foundation of China [21971196]
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A novel and straightforward approach for the synthesis of tribenzo[b,d,f]azepines has been developed from 2-iodobiphenyls and 2-bromoanilines. A wide range of products were obtained via a cascade intermolecular palladium-catalyzed C-H activation/dual coupling reaction, with C,C-palladacycles likely being the reaction intermediates.
A novel and straightforward approach for the synthesis of tribenzo[b,d,f]azepines starting from 2-iodobiphenyls and 2-bromoanilines has been developed. A wide range of tribenzo[b,d,f]azepines were obtained in good to excellent yields via a cascade intermolecular palladium-catalyzed C-H activation/dual coupling reaction. C,C-palladacycles, which are generated by C-H activation of 2-iodobiphenyls, should be the reaction intermediates.
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