4.7 Article

Microstructure evolution and tensile properties of as-rolled TiB/TA15 composites with network microstructure

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2021.140783

Keywords

Titanium matrix composite; Network microstructure; TiB; Silicide; Hot rolling; Tensile properties

Funding

  1. National Key R&D Program of China [2017YFB0703100]
  2. Key-Area Research and Development Program of Guang Dong Province [2019B010942001]
  3. National Natural Science Foundation of China (NSFC) [51731009, 51822103, 51901056]
  4. Fundamental Research Funds for the Central Universities [BRETIV.201902, HIT.NSRIF.2020002]

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TiB whiskers reinforced Ti-6.5Al-2Zr-1Mo-1V (TA15) composites with the addition of silicon element and different TiB volume fractions were successfully fabricated and rolled in the alpha+beta region, showing improved room-temperature properties. The increase in strength was attributed to grain refining of the matrix, directional distribution of TiB whiskers, and hinder of silicides, while the enhancement in ductility was due to increasing matrix connectivity, grain refining, and bimodal microstructure DRX behavior. At high temperatures, the tensile strengths increased significantly after rolling, attributed to directional distribution of TiB whiskers, grain refining, and larger silicides. The highest strengths achieved were 820 MPa at 600°C and 698 MPa at 650°C.
To investigate the microstructure evolution and mechanical properties of DRTMCs with network microstructure during the rolling deformation, the TiB whiskers reinforced Ti-6.5Al-2Zr-1Mo-1V (TA15) composites (TiBw/ TA15) with the addition of silicon element and different TiB volume fractions were successfully fabricated by hot pressing sintering and rolled in the alpha+beta region. Compared with the as-sintered composites, the as-rolled composites presented the lower local TiBw content, higher matrix connectivity, remarkable grain refining and larger silicides. After rolling deformation, the room-temperature ultimate strength and fracture elongation were dramatically improved. The as-rolled 3.5 vol.% TiBw/TA15 composite obtained better combination properties of 1248 MPa and 10.5% at room temperature. The increase in strength can be attributed to grain refining of the matrix, directional distribution of TiBw, and stronger hinder of silicides. The enhancement of ductility was due to increasing matrix connectivity, grain refining as well as DRX behavior of bimodal microstructure. As for high temperature properties, the tensile strengths increased by 26-32% at 600 degrees C and 20-32% at 650 degrees C after rolling, which is also attributed to directional distribution of TiBw, grain refining of matrix and larger silicides. The highest strengths at 600 degrees C and 650 degrees C are 820 MPa and 698 MPa, respectively. The fracture behavior of the composites was discussed in detail.

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