4.7 Article

Fully coupled electrothermal and mechanical simulation of the production of complex shapes by spark plasma sintering

Journal

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
Volume 41, Issue 7, Pages 4252-4263

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2021.02.010

Keywords

Spark plasma sintering; Numerical modelling; Complex shapes; Creep parameters

Funding

  1. Norimat
  2. Association Nationale Recherche Technologie (ANRT)as part of the CIFRE (Industrial Agreement of Formation by Research) [2017/1026]
  3. Programme Operationnel FEDER-FSE Midi-Pyrenees et Garonne 2014-2020as part of the CERAPRINT project [17014462]

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Creep parameters for Al2O3 and TiAl samples were determined through numerical identification, with the resulting mechanical model coupled with an electro-thermal model for a fully coupled simulation of SPS. This simulation accurately predicts density gradients and interface distortion during sintering, making it an efficient tool for obtaining fully dense objects with desired geometry.
The obtention of an accurate mechanical model of the spark plasma sintering (SPS) requires the identification of creep parameters. Those parameters are usually determined experimentally, which involves several tests and could be a source of error for the model predictions. A numerical identification, based on only one SPS experiment per material, allowed the determination of the creep parameters of Al2O3 and TiAl samples. The resulting mechanical model was then coupled with an electro-thermal model of the system to obtain a fully coupled simulation of the SPS. This model can predict the densification behavior not only of simple pellets, but also of complex shape configurations. It accurately predicts the density gradients inside the complex sintered parts as well as the interface distortion during sintering. Thus, numerical simulation can be used as an efficient predictive tool to obtain fully dense objects with the desired geometry.

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