Journal
JOURNAL OF ALLOYS AND COMPOUNDS
Volume 856, Issue -, Pages -Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2020.158140
Keywords
Yttrium iron garnet; Consecutive precipitation; Crystalline structure; Particle morphology; Magnetization; Ferromagnetic resonance
Categories
Funding
- National Academy of Sciences of Ukraine [0120U102727, 0119U100469]
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In this study, a method for synthesizing nanosize particles of Y3AlFe4O12 garnet ferrite by precipitation in aqueous solutions at constant pH has been demonstrated. It was found that the filtration coefficient is three times greater when iron and aluminum hydroxides are precipitated simultaneously compared to when all hydroxides are precipitated simultaneously. After treatment at 800 degrees C, crystalline nanoparticles with an average particle size of 60-70 nm are formed. The ceramics obtained after proper heat treatment exhibit high density and good electrophysical properties.
A method to synthesize nanosize particles of Y3AlFe4O12 garnet ferrite by precipitation in aqueous solutions at constant pH during the synthesis has been demonstrated. The effect of the sequence of the metal hydroxides precipitation on the filtration coefficient is studied. The filtration coefficient is found to be three times greater in the case of simultaneous precipitation of iron and aluminum hydroxides compared to the one observed for the case of simultaneous precipitation of all hydroxides. Synthesized precipitates are established to be amorphous and crystalline nanoparticles are formed in one stage after the treatment at 800 degrees C. The average particles size is around 60-70 nm. The ceramics obtained after a proper heat treatment of the nanoparticles is shown to be characterized by the high density and good electrophysical properties. (C) 2020 Elsevier B.V. All rights reserved.
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