Journal
ELECTROPHORESIS
Volume 37, Issue 22, Pages 3017-3019Publisher
WILEY-BLACKWELL
DOI: 10.1002/elps.201600265
Keywords
Boron isotope; Boron neutron capture; Capillary electrophoresis; Enriched boric acid; Isotopic separation
Funding
- Russian Science Foundation [16-13-10117]
- Russian Science Foundation [16-13-10117] Funding Source: Russian Science Foundation
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Fast isotopic separation of B-10 and B-11 boric acid by CZE was demonstrated. The BGE contained 25 mM phenylalanine and 5 mM putrescine (pH 8.95). The running conditions were +25 kV at 20 degrees C with indirect photometric detection at 210 nm. Baseline separation was achieved in less than 9 min. RSD of migration times and corrected peak areas were less than 0.5 and 3%, respectively (n = 5). Linearity was demonstrated in the range 0.22 mM for B-11 and 0.2-0.5 mM for B-10.
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