Journal
POLYHEDRON
Volume 193, Issue -, Pages -Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.poly.2020.114896
Keywords
Palladium; Sandwich Polyoxometalate; Hydrogenation; Nitrobenzene
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Funding
- Science and Engineering Research Board (SERB), New Delhi [EMR/2016/005718]
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The study successfully synthesized a tri-palladium substituted sandwich type phosphotungstate and supported the crystal data with various spectral analysis. A preliminary study showed the catalytic activity of the complex in the hydrogenation of nitrobenzene.
The present work showcases, first time, the synthesis of tri-palladium substituted sandwich type phosphotungstate, [Pd-3(PW9O34)(2)](11-), from its individual salts in super acidic medium as well as the single crystal structure of the same. Further, various spectral analysis carried out to support the crystal data. A preliminary study for the hydrogenation of nitrobenzene has been carried out to evaluate the catalytic activity of the complex. (C) 2020 Published by Elsevier Ltd.
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