Realizing superior ductility of selective laser melted Ti-6Al-4V through a multi-step heat treatment

The use of selective laser melting (SLM) has become more common with regard to the fabrication of high-strength Ti-6Al-4V components. However, the as-SLMed Ti-6Al-4V alloy parts typically exhibit low ductility because of the formation of acicular and brittle alpha' martensites. It is essential to use post-heat treatment to change their microstructures to achieve superior mechanical properties. In this study, a particular multi-step heat treatment (MSHT) was applied to the Ti-6Al-4V alloy samples fabricated via SLM. Conventional post-heat treatments were conducted for comparison. The microstructures and tensile properties of the as-SLMed and heat-treated samples were investigated. The as-SLMed Ti-6Al-4V sample is dominated by plate and acicular alpha' martensites, which exhibit high strength (1280 MPa) and low ductility (9.0%). The conventional solution plus aging or stress-relieving treatment cannot result in a good combination of strength and ductility. A single step annealing process at 700 degrees C for 2 h changes the martensitic structure to a fine lamellar alpha+beta structure, which provides a strong and ductile Ti-6Al-4V with an ultimate tensile strength of 1108 MPa and a total elongation of 17.6%. In contrast, the MSHT process facilitates the globularization of alpha and, thereby generates a nearly equiaxed structure, resulting in superior ductility (21.8% of total elongation), while maintaining a moderate ultimate tensile strength of 953 MPa.

Automated summary

The study found that a single-step annealing process can change the martensitic structure to a fine lamellar α + β structure, providing a Ti-6Al-4V alloy with high strength and ductility. In contrast, the multi-step heat treatment process facilitates the globularization of the α phase, creating an almost equiaxed structure with superior ductility while maintaining a moderate ultimate tensile strength.