Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 240, Issue -, Pages -Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2020.109670
Keywords
PhIO/HF center dot THF reagent; Electrophilic fluorination; Hydrogen fluoride; Hypervalent iodine; Fluorination reagents
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Funding
- National Natural Science Foundation of China [21761132021]
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New electrophilic fluorination reagent HF center dot THF/PhIO was introduced and tested on three general classes of compounds. Compared with the literature data reported for basic reagents, such as HF/TEA/PhIO and HF/Py/PhIO, the new reagent showed superior performance in fluorination of aromatic alkenes, subpar reactivity with ketones and malonates, while in the reactions with 1,3-unsaturated carbonyl compounds the results were much the same as the literature data.
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