Characteristic and mechanism of dynamic recrystallization in a newly developed Fe-Cr-Ni-Al-Nb superalloy during hot deformation

Thermal-mechanical experiments of a newly developed Fe-Cr-Ni-Al-Nb superalloy were conducted on a Gleeble simulator under the temperature of 900-1100 degrees c and the strain rate of 0.01-5 s(-1). The microstructure evolution and the nucleation mechanisms of dynamic recrystallization (DRX) were characterized by electron backscattering diffraction (EBSD) technique, and the results showed that relatively higher temperature, lower strain rate and larger true strain were favorable for DRX. When the superalloy was deformed under 1050 degrees c- 0.1 s(-1), nearly complete DRX occurred with the power dissipation efficiency of 0.34. Moreover, the Avrami dynamic model of the investigated superalloy was constructed, which suggested that there were three stages during DRX, including nucleation, grain growth and grain contact. Furthermore, three different DRX mechanisms during hot deformation were identified. The bulge and nucleation characteristics of original grain boundaries occurred within all experimental parameters, confirmed that discontinuous dynamic recrystallization (DDRX) was the main DRX mechanism. Besides, the presence of a small amount of medium angle grain boundaries affirmed that subgrains continuously rotated and absorbed dislocations during deformation, meaning that the continuous dynamic recrystallization (CDRX) was an auxiliary nucleation mechanism. Moreover, annealing twins, appeared in the matrix, provided additional nucleation sites for DDRX and CDRX, encouraging the twinning dynamic recrystallization (TDRX), which effectively promoted the progress of DRX. (C) 2021 Elsevier B.V. All rights reserved.

Automated summary

The thermal-mechanical experiments on a newly developed Fe-Cr-Ni-Al-Nb superalloy revealed that higher temperature, lower strain rate, and larger true strain were favorable for dynamic recrystallization. The study also identified three stages during dynamic recrystallization and three different mechanisms for the process.