Journal
CERAMICS INTERNATIONAL
Volume 47, Issue 9, Pages 12789-12794Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.01.139
Keywords
Joining; Interfaces; MgO
Categories
Funding
- Advanced Characterization Nanotechnology Platform, Nanotechnology Platform Program of the Ministry of Education, Culture, Sports, Science and Technology (MEXT), Japan at the Research Center for Ultra-High Voltage Electron Microscopy (Nanotechnology Open Fa [JPMXP09A20OS0022]
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The surfaces of Al2O3 ceramic plates were metallized using a friction stir spot welding method, showing good adhesive strength. Investigation revealed the formation of a microcrystalline MgO layer at the interface, leading to strong adhesion. Bonding two metallized Al2O3 ceramic plates together at 1100 °C under vacuum resulted in a strong cross tensile strength, indicating strong adhesion.
The surfaces of Al2O3 ceramic plates were metallized with by a friction stir spot welding method. Tensile tests revealed that the adhesive strength between the Mg film and Al2O3 ceramic plate was 23.3 MPa. To investigate the origin of this strong adhesion, the interface structure was examined by X-ray diffraction, scanning transmission electron microscopy?energy-dispersive X-ray spectroscopy, and transmission electron microscopy. The results indicated the formation of a microcrystalline MgO layer at the interface. Furthermore, the surfaces of two metallized Al2O3 ceramic plates separated by Ni foil were bonded together by hot pressing at 1100 ?C for 180 min under vacuum. The resulting cross tensile strength of the bonding was 2.1 MPa, indicating strong adhesion between the Al2O3 ceramic plates.
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