Journal
BULLETIN OF MATERIALS SCIENCE
Volume 43, Issue 1, Pages -Publisher
INDIAN ACAD SCIENCES
DOI: 10.1007/s12034-020-02117-3
Keywords
PbFCl; BaFCl; layered material; exfoliation; supercapacitor
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Funding
- ICMS
- SSL
- TRC
- JNCASR
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Two-dimensional layered PbFCl and BaFCl have been prepared by solid-state reactions and the crystal structures were subjected to Rietveld refinement to obtain structural parameters. The compounds characterized by several methods including X-ray photoelectron spectroscopy, X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy, etc. have been subjected to ultrasonic exfoliation in different solvents such as water, dimethylformamide and N-methyl-2-pyrrolidone. Water is found to yield single layers of both these halides. The supercapacitor performances of PbFCl, BaFCl and the exfoliated materials have been studied. Exfoliated 1-2 layered PbFCl exhibits a high-specific capacitance of 158 F g(-1) at a scan rate of 10 mV s(-1).
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