Journal
SYNLETT
Volume 31, Issue 19, Pages 1907-1912Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0040-1707281
Keywords
nitrosation; oximes; flow chemistry; Toray process; photochemistry
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The nitrosation of several alkanes using tert- butyl nitrite has been performed in flow showing a remarkable reduction in the reaction time compared with batch processing. Due to the necessity for large excesses of the alkane component a continuous recycling process was devised for the preparation of larger quantities of material.
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