Journal
CRYSTENGCOMM
Volume 18, Issue 28, Pages 5257-5261Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ce00375c
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Funding
- Natural Science Foundation of China [21303038]
- Open Funds of the State Key Laboratory of Rare Earth Resource Utilization [RERU2016004]
- Scientific Research Foundation for the Returned Overseas Chinese Scholars-SEM
- 100 Talents Program of Anhui Province
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To obtain bulk cubic CH3NH3PbI3, chlorobenzene was employed to regulate the CH3NH3PbI3 gamma-butyrolactone solution with high saturated solubility at room temperature and a high yield of crystal at 60 degrees C. As a result, bulk cubic CH3NH3PbI3 single crystal was successfully synthesized for the first time in mixed-solvent method at 60 degrees C, which is a little higher than the tetragonal-cubic phase inversion temperature.
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