Journal
ORGANIC LETTERS
Volume 22, Issue 20, Pages 7864-7869Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c02770
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Funding
- National Research Council of Thailand (NRCT) [NRCT5-RSA63001-16]
- Thailand Research Fund [RTA6180007]
- National Nanotechnology Centre (NANOTEC), NSTDA, Ministry of Science and Technology, Thailand, through its program of the Centre of Excellence Network
- Science Achievement Scholarship of Thailand
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In this work, we developed the catalytic guanylation of thiourea using Ru(bpy)(3)Cl-2 as a photocatalyst under irradiation by visible light. The conversion of various thioureas to the corresponding guanidines was achieved using 1-5 mol % of photocatalyst in a mixture of water and ethanol at room temperature. Key benefits of this reaction include the use of photoredox catalyst, low-toxicity solvents/base, ambient temperature, and an open-flask environment.
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