Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 85, Issue 18, Pages 11892-11901Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.0c01688
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Funding
- National Natural Science Foundation of China [21672174, 21977084]
- Natural Science Foundation of Chongqing [cstc2019jcyj-msxmX0297]
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A novel method for the synthesis of benzo[4,5]imidazo[2,1-a]isoquinolin derivatives via visible-light-induced radical cascade cyclization is described. By using N-methacryloyl-2-phenylbenzoimidazoles and diverse radical precursors, various benzo[4,5]imidazo[2,1-a]isoquinolin derivatives containing CH2CN/CF2COOEt/CF3 can be formed in good to excellent yields under mild reaction conditions. This method exhibits good functional group tolerance and a wide range of substrate scope.
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