4.7 Article

Influence of fibres diameter on the AC and DC magnetic characteristics of Fe/Fe3O4 fibres based soft magnetic composites

Journal

CERAMICS INTERNATIONAL
Volume 47, Issue 2, Pages 1865-1874

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2020.09.015

Keywords

Soft magnetic composites; Fibres-based composites; Fe3O4 coating; Fibres diameter; Loss separation

Funding

  1. Romanian Ministery of Research and Innovation, CNCS-UEFISCDI [PN-III-P1-1.1-TE-2016-0649]

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Fibres-based soft magnetic composites (FSMCs) were prepared using Fe fibres of different diameters coated with Fe3O4, leading to significant improvements in magnetic properties. Thinner fibers result in composites with low losses and stable initial permeability in a specific frequency range.
Fibres-based soft magnetic composites (FSMCs) have been prepared by using Fe fibres of different diameters (65, 125, 250 and 500 mu m). The Fe fibres were coated with a 3 mu m thick layer of Fe3O4 via the blackening process and subsequently compacted at 700 MPa. The X-ray diffraction analysis (XRD) was used to prove the formation of the Fe3O4 coating on the surface of the fibres. The thickness and the uniformity of the coating were analysed via scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX). The DC measurements performed on the composite cores revealed that the saturation induction increase from 1.36 to 1.68 T, the maximum relative permeability increase from 550 to 940, and the coercive field decrease from 796 to 454 A/m as the fibre's diameter increase from 65 to 500 mu m. By using thinner fibres (65 and 125 mu m), composites with low losses and stable initial relative permeability, in the frequency range 50 Hz-10 kHz, can be obtained. To distinguish between different types of losses dissipated by our compacts, and the influence of the fibre's diameter on the different components of the total losses, a numerical model for loss separation is proposed. The comparative evolution of the AC magnetic characteristics of the FSMCs and powder-based SMCs is presented. According to the presented results, this new type of composites can be successfully used to prepare magnetic cores designated to work in the medium to high-frequency range.

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