4.7 Article

Microstructure and texture evolution of fine-grained Mg-Zn-Y-Nd alloy micro-tubes for biodegradable vascular stents processed by hot extrusion and rapid cooling

Journal

JOURNAL OF MAGNESIUM AND ALLOYS
Volume 8, Issue 3, Pages 873-882

Publisher

KEAI PUBLISHING LTD
DOI: 10.1016/j.jma.2019.09.012

Keywords

Magnesium alloy; Micro-tube; Microstructure; Rapid cooling; Texture

Funding

  1. Key Projects of the Joint Fund of the National Natural Science Foundation of China [U1804251]
  2. National Key Research and Development Program of China [2018YFC1106703, 2017YFB0702504, 2016YFC1102403]

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Magnesium alloys have narrow available slip result from close-packed hexagonal structure that limit their processing properties. In the recent work, the Mg-2Zn-0.46Y-0.5Nd, as materials for degradable stents, was applied to produce as-extruded micro-tube with an outer diameter of 3.0 mm and a wall thickness of 0.35 mm by hot extrusion with an extrusion ratio of 105:1 at 653 K and rapid cooling. The fine microstructure of the dynamic recrystallization of as-extruded micro-tube could be preserved by rapid cooling such as water-cooled, resulting in more excellent mechanical properties relative to air-cooled micro-tube. The addition of rare earth elements Y and Nd results in continuous dynamic recrystallization dominated the dynamic recrystallization mechanism. During the hot extrusion process, the activation of the non-basal slip system, especially the pyramidal < c + a > slip, could significantly weaken the texture strength, and the as-extruded micro-tube exhibits weak RE texture components < 01 (1) over bar1 > parallel to ED and <(1) over bar2 (1) over bar1 > parallel to ED. Hence, the magnesium alloy micro-tube prepared by the rapid cooling has fine microstructure and weak texture, which is favorable for further process and governance. (c) 2020 Published by Elsevier B.V. on behalf of Chongqing University.

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