Journal
ACS SUSTAINABLE CHEMISTRY & ENGINEERING
Volume 8, Issue 29, Pages 10740-10746Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acssuschemeng.0c02289
Keywords
visible light-induced; g-C3N4-catalyzed; decarboxylative reaction; solvent-dependent system
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Funding
- Center of Advanced Analysis & Computational Science (Zhengzhou University)
- National Natural Science Foundation of China [21501010, 21971224]
- Key Research Projects of Universities in Henan Province [18B350008, 20A150006]
- Henan Province Young Talents Elevation Program [2019HYTP023]
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An effective and simple visible light-induced heterogeneous g-C3N4-catalyzed decarboxylative reaction of quinoxalin-2(1H)-ones with N-aryl glycines was developed. When the reaction was performed in DMSO/H2O and EtOH, the products dihydroquinoxalin-2(1H)-ones and tetrahydroimidazo[1,5-a]quinoxalin-4(5H)-ones were unprecedentedly obtained in good yields, respectively. This solvent-dependent system offers advantages, including simple and easy operation, short reaction time, high chemoselectivity, a recyclable catalyst, metal-/base-/oxidant-free, and mild reaction conditions.
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