Journal
ORGANIC LETTERS
Volume 22, Issue 15, Pages 5910-5914Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c02008
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Funding
- National Natural Science Foundation of China [21971110, 21732003]
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The remote C(sp(3))-H cyanation of carboxamides has been described by merging photoredox and copper catalysis in a site-selective and enantiocontrolled manner. The protocol is the integration of photoinduced and nitrogen-centered radical-mediated intermolecular hydrogen atom transfer with chiral copper-complex-catalyzed radical cyanation. This strategy gives enantio-enriched cyanated amides in high yields.
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