Journal
CHINESE JOURNAL OF CHEMISTRY
Volume 38, Issue 10, Pages 1203-1204Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cjoc.202000256
Keywords
Spirosilabiindane; Hydrosilation; Ligands; SPSiOL; SPSiPhos
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We report the development of a class of chiral spirosilabiindane scaffoldsviaRh-catalyzed asymmetric double hydrosilation. Enantiopure SPSiOL (spirosilabiindane diol), a new type of chiral building block for preparation of various chiral ligands and catalysts, could be readily prepared on >10-gram scale using this protocol.
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