Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 26, Issue 68, Pages 15847-15851Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.202003430
Keywords
carbazoles; electrochemistry; green chemistry; heterocyclic chemistry; N; C coupling
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Funding
- Deutsche Forschungsgemeinschaft [WA 1276/17-2]
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A constant current protocol, employing undivided cells, a remarkably low supporting electrolyte concentration, inexpensive electrode materials, and a straightforward precursor synthesis enabling a novel access to N-protected carbazoles by anodic N,C bond formation using directly generated amidyl radicals is reported. Scalability of the reaction is demonstrated and an easy deblocking of the benzoyl protecting group is presented.
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