Journal
CHEMISTRYSELECT
Volume 5, Issue 13, Pages 3847-3849Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/slct.201904510
Keywords
Electrolysis; Hydrazides; Nitriles; One pot synthesis; 1; 2; 4-Triazoles
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A highly facile, efficient and environmentally friendly protocol for the first electrochemical synthesis of 3, 5-disubstituted 1, 2, 4-triazoles from nitriles and hydrazides is reported. The reaction efficiency involves anodic oxidation and cathodic reduction, and has a good functional group tolerance. This synthetic approach is operationally simple and gives good to excellent yields under mild conditions in a one-pot procedure. It utilizes KI as the redox catalyst under external oxidant-free conditions.
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