Journal
CHEMISTRY-AN ASIAN JOURNAL
Volume 12, Issue 1, Pages 130-144Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/asia.201601413
Keywords
acetoxylation; C-H activation; olefination; phenols; regioselectivity
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Funding
- National Natural Science Foundation of China [NSFC-21272185, 21572178]
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An efficient palladium(II)-catalyzed intermolecular direct ortho-alkenylation and acetoxylation of phenols has been developed. The reaction proceeded via a seven-membered cyclopalladated intermediate and showed complete regio- and diastereoselectivity. The approach also provided an efficient route for the synthesis of coumarins and benzofurans.
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